3. Considering the techniques and instrumentation used to perform these experiments, identify 2 potential sources of error if you were to repeat this experiment in the "real world". Human error is not an acceptable answer. Discuss at least two possible sources of error that could contribute to your percent error. A student is performing Reaction 2 and does not completely dissolve the NaOH pellets before acquiring the final temperature. How will this affect his value for AH, and his percent error calculations?
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- suppose your absent minded lab partner grabbed medium porosity filter paper instead of the fine porosity paper and you noticed cloudiness in your filtrate. will the reported concentration of limiting reactant solution be greater than, less than, or equal to the true concentration of limiting reactant solution? Na3PO4 and BaCl2 are the solutions usedFor a strong acid with a strong base neutralization reaction, does the reactant 1 : reactant 2 : product always have a coefficient ratio of 1 : 1 : 1? Why is that?Please do not answer if you will not respond to this question.C. Purification of Water 1.For this part of the experiment, watch the video on the link(s) below: a. Flocculation: https://www.youtube.com/watch?v=5uuQ77vAV_U&t=82s Question: Observation before flocculation. Observation after Flocculation
- Using the percent purity calculations, determine the percent yield of synthesis of aspirin. Part I Synthesis of Aspirin Mass of salicylic acid used (g) 2.029g Volume of acetic anhydride used (mL) 5ml Mass of acetic anhydride used (vol. × 1.08 g/mL) 5.4g Mass of aspirin synthesized (g) 3.256g Part II Melting Temperature Data Melting temperature (°C) 133°C Part III Salicylic Acid Standard Stock Solution Initial mass of salicylic acid (g) 0.210g Moles of salicylic acid (mol) 0.0147 mol Initial molarity of salicylic acid (M) 0.724 M Part III Beer’s Law Data for Salicylic Acid Standard Solutions Trial Concentration (M) Absorbance Water (mL) 1 10 0.301 0 2 7.5 0.219 2.5 3 5.0 0.163 5.0 4 2.5 0.074 7.5 Best-fit line equation for the salicylic acid standards Test of the Purity of the Synthesized Aspirin Initial mass of aliquot of product (g)…Preparation of 0.25N NaOH Objective: Apparatus and Materials: Procedure : Calculate the exact mass of NaOH needed to prepare 1.0L of 0.25N NaOH for standardization. Show your computations. Using the triple beam balance, weigh the desired amount of NaOH. Place the weighed amount of NaOH into the 500 mL volumetric flask and add distilled water until it reaches the mark. Agitate and transfer the solution into the reagent bottle. Add again distilled water to the same volumetric flask until it reaches the mark and pour it to the same reagent bottle, thus having a total volume of 1.0 L. Label the reagent bottle, 0.25N NaOH. Data and Computations: Conclusion:One way to determine the hardness of a water sample is to precipitate the calcium out of solution as a carbonate. The net ionic reaction for this precipitation is: Ca2+(aq) + CO32-(aq) → CaCO3 (s) A 1.00 L sample of water is drawn from a Phoenix, AZ well and 0.534 g of calcium carbonate is recovered using the above reaction. What was the Ca2+ concentration of the original water sample in ppm? Show your work and include units. Hint: ppm stands for parts per million, and in the case of an aqueous solution, this is equivalent to mg/L.
- If an instrument gives a response of 1240 for a standard containing 8 ppm of a substance, how much if this substance is in a sample that gives a response of 1705? Are any assumptions needed?How would each of the following errors affect the determination of the molar mass of the unknown (Increase/Decrease/No effect)? a. Thermometer reads 2.0o higher than the true temperature. b. Some of the t-butanol was unknowingly spilled after it had been weighed but before the solute was added. 3. A student accidentally added acetylsalicylic acid (MW = 180.157 g/mol) rather than salicylic acid (MW = 138.121 g/mol), if no other mistakes were made, how would this error affect the determined molal freezing point depression constant for t-butyl alcohol (Kf)? 4. Based on the Tf and Kf you determined for t-butyl alcohol, predict the freezing point of a t-butyl alcohol solution containing 0.530 m NaCl. Assume 1.9 is the van’t Hoff factor for NaCl in t-butyl alcohol. Show your work.How to find the 'K" value using the date in the tables for experiments 1-4
- Check out the following video and write the balanced equation in this question. Hint: Remember to first determine the reaction type and then write products. All ions will have the same charge in the reactants and products. You'll need your solubility rules for this one! Please make sure to use phases for each substance and parentheses (when needed) and subscripts. https://www.youtube.com/watch?v=X2mB-q2NQXY&feature=emb_title (37 second video)By the use of Henderson Hasselbalch equation; pH = pKa + log{[acetate ion]/[acetic acid]} 4.5 = 4.75 + log{[0.10 M]/[acetic acid]} -0.25 = log{[0.10 M]/[acetic acid]} [Acetic acid] = 0.10 M/ 10-0.25 [Acetic acid] = 0.10 M/0.56 [Acetic acid] = 0.1786 M Moles of sodium acetate dissolved in 250 mL buffer solution = 0.10 M× (250mL/1000mL) × 1L = 0.025 mol Weight (w) of sodium acetate (purity 100%) dissolved to prepare 250 mL of solution with buffer concentration of 0.10 M is calculate as follow; w100% = 0.025 mol × 82.0343 g/mol = 2.051 g Weight (w) of sodium acetate (purity 99%) is calculate as follow; w99% = 2.051 g× (100/99) = 2.072 g What was the volume of 6.12 M acetic acid HC2H3O2 needed to prepare the 250 mL acetic acid/acetate ion buffer solution required in this part? Show your calculations.Compare and contrast an anticipatory standard to a reactionary standard by listing and describing some advantages and disadvantages.