8. 1. КОН, НО, heat Ме Me H. 2. EtMgBr, THF 3. РСС, СH,Cla 4. MeLi, Cul, THE 9. Br 1. Pd°Ln, EtgN, MECN, Me 2. mCРBА, СH2Clz 3. HCIO, ELOH Me CO,Me 10. 11. OMe Me , NaH, THF 1. Ph P BrO 12. 2. NaOH, H2O2, H2O/THF 3. MegS , ÑaH, THF H.

Principles of Instrumental Analysis
7th Edition
ISBN:9781305577213
Author:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Chapter30: Capillary Electrophoresis, Electrochromatography, And Field-flow Fractionation
Section: Chapter Questions
Problem 30.12QAP
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8.
1. КОН, Н,О, heat
Me
Me
H.
2. EtMgBr, THF
3. РСС, СН,Cl
4. MeLi, Cul, THE
9.
Br
1. Pd°Ln, EtgN, MeCN,
Me
2. mCPBА, СH,Clk
3. HCIO, ELOH
Me
CO,Me
10.
11.
OMe
Me
, NaH, THF
1. Ph3P
BrO
12.
2. NaOH, H,O2. Н.ОТHF
3. Megs , NaH, THF
H.
Transcribed Image Text:8. 1. КОН, Н,О, heat Me Me H. 2. EtMgBr, THF 3. РСС, СН,Cl 4. MeLi, Cul, THE 9. Br 1. Pd°Ln, EtgN, MeCN, Me 2. mCPBА, СH,Clk 3. HCIO, ELOH Me CO,Me 10. 11. OMe Me , NaH, THF 1. Ph3P BrO 12. 2. NaOH, H,O2. Н.ОТHF 3. Megs , NaH, THF H.
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