A company illegally dumped their wastewater on a river bank. You are part of an environmental NGO that are tasked to determine what kind toxins that may have contaminated the waters. What kind of analysis would you do? a. Characterization analysis b. Qualitative analysis c. Fundamental analysis d. Quantitative analysis
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1. A company illegally dumped their wastewater on a river bank. You are part of an environmental NGO that are tasked to determine what kind toxins that may have contaminated the waters. What kind of analysis would you do?
a. Characterization analysis
b. Qualitative analysis
c. Fundamental analysis
d. Quantitative analysis
2. Four groups weighed ten rock samples each, and tested the possibility of outliers using Q-test. At 95.0% confidence (a = 0.05), which of the following is considered to be an outlier?
a. 0.024
b. 0.413
c. 0.453
d. 0.674
3. An unknown solution containing oxalic acid, which is a diprotic acid, is titrated against sodium hydroxide. How many mole/s of titrant is needed to react with one mole of analyte?
a. ½
b. ¼
c. 2
d. 4
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- Assignment: This is an individual activity. After studying the lesson and watching all the videos, answer the following questions. Answer in not more than 3 sentences per question. 1. Discuss the a) direct method of weighing b) indirect weighing using the analytical balance. 2. Explain how suction filtration is carried out in the laboratory. Give the important points that must be observed in doing the process. 3. Explain why it is important to wash the precipitate. Can distilled water be used to wash all types of precipitates? 4. Discuss how to use a desiccator. When should a desiccant be replaced?Explain the use of plans and their importance in assessing the quality of pharmaceutical products. Provide a step-by-step design of a sampling plan based on a normal inspection for a 75,000 tablets with an AQL of 0.12% using the attached table (at the end of exam paper).1. A student performed this experiment and obtained the following concentration values: 0.02813 M, 0.02802, and 0.02788 M a. what is the mean concentration? b. what is the standard deviation of these results? 3. how would the following errors affect the concentration of Cl- obtained in question 2b? give your reasoning in each case. a. the student read the molarity of AgNo3 as 0.02104M instead of 0.02014M b. the student was past the endpoint of titration when he took the final buret reading.
- Analytical chemistry is a particular field within the broader spectrum of the chemical sciences, in which many times the focus of analytical experiments is to develop new methods to analyze compounds, either structurally or by determining concentrations of compounds. One of the processes analytical chemists use to determine the exact concentration of a working solution is called standardization. In your own words, describe the differences between a primary, secondary, and tertiary standard, and describe the underlying concept behind the standardization process. Why is it done?1. Which of the following is not a step in preparing a water sample container?a. All sample containers must be dark in colorb. The type of sample container and the level of cleaning required depend on the type of sample to be takenc. All sample containers must be thoroughly cleaned in the laboratory before sampling is carried outd. The number of containers prepared must always be in excess of what is needed, for quality assurance, quality control and reserves 2. The purpose of environmental sample analysis is..a. To determine the origin and concentration of chemicals in the environmentb. To determine the origin, concentration of chemicals and/or pollutants in the environmentc. To determine the concentration of a chemical in the environmentd. To determine the cause and concentration of pollutants in the environment1. why is statistics itself is important in the field of chemistry especially in analytical chemistry? 2.Differentiate random errors from systematic errors. Give three examples each of these type of errors in titrimetric analysis.
- 1. Explain both precision and accuracy as they pertain to chemical measurements. 2. Why would you use the method of standard addition to calibrate a measurement instead of a calibration curve?What are the differences between systematic and random errors and how do they effect accuracy and precision? In what circumstances would you use standard addition (versus a normal calibration curve) to determine the amount of an analyte in a sample? A urine sample, containing analyte Z is analysed by the standard addition method where 5 mL of the original sample was mixed with increasing amounts of a Z standard and each solution diluted to a volume of 50 mL prior to analysis. A plot of the final concentration of the standard in each of the 50 mL samples (x axis) versus The measured signal from the analysis of each 50 mL sample (on y axis) produced a straight line with the general equation: y = 44.72x + 4.06 what was the final concentration of Z in the 50 mL standard addition sample? what was the initial concentration of Z in the original urine sample?For EACH type of gravimetric analysis:Give actual applications of each analysis. Include the SPECIFIC methodology for each sample chosen.
- You determine the acetic acid (HOAc) content of vinegar by titrating with a sodium hydroxide standard solution to a phenolphthalein (an indicator) end point. An approximately 5-mL sample of vinegar is weighed on an analytical balance in a weighing boat and this is found to be 5.0268 g. The standard deviation in making a single weighing is 0.2 mg. The sodium hydroxide must be accurately standardised (this means its concentration must be accurately determined) by titrating known mass of high-purity potassium hydrogen phthalate, and three such titrations give molar concentrations of 0.1167, 0.1163 and 0.1164 mol L-1. A volume of 36.78 mL of sodium hydroxide is used to titrate each sample. The standard deviation of the burette used is 0.02 mL. Calculate the percentage of acetic acid in the vinegar and its standard deviation.A dilution of benzene in methanol is made by placing 1.5 mL benzene (density of benzene is 0.879 g/mL and its mol. Wt. is 78.1) in a 100-mL volumetric flask and brining to volume with methanol. What is the concentration of benzene in the solution in mg/L In ppmlA calibration curve of KCl conductivity (y-axis) vs concentration (mass percent, x-axis) is made. The equation of line of best fit is y = 578.3x + 0.380 and the R 2 is 0.9998. Based on this data what is the mass percent of an unknown KCl solution with a conductivity of 2,788 uS/cm? 6.55 % 6.12 % 4.14 % 3.98 % 4.82 %