A crucible and its cover weigh 65.82 grams. You add a hydrate of a salt and it now weighs 83.77 g heat the crucible, cover slightly ajar, until the contents are completely dry and it now weighs 81.06 9, 10. Calculate the experimental percent water in the sample in this hydrate. 11,12.Calculate the theoretical percent of water for the compound FeSO, 7H20
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- 125.1 mg of streptomycin sulphate are dissolved in 10 ml of water. A GC headspace analysis is carried out in order to determine the methanol content of the drug. A peak for methanol is produced which has 73.2% of the area of a peak for a methanol standard containing 0.532 mg/100 ml of methanol in water analysed under exactly the same conditions, What is the methanol content of the streptomycin sulphate in ppm and %w/w? Answer: 311.3 ppm, 0.3113 % w/w.how??10g coffee 4g sodium carbonate 40m dichloromethane 160ml distilled water coffee filter What are the principles behind caffeine being extracted from coffee using the above items? 1st sodium carbonate mixed with coffee then brought to a boil for 20min then solution/grinds are filtered. Then solution is added to a separatory funnel with 15ml of dichloromethane and two layers are observed so the bottom layer with DCM contains the caffeine, then this layer is collected in a beaker and dried out using molecular seeds. Then the solvent is brought to a boil with crude caffeine remaining and recystallized using 95% ethanol and brought to a boil again. Then the contents are vaccum filtered and allowed to dry resulting in 30mg caffeine.The gravimetric factor used to express CoCBr6·H20 in a sample that is finally weighed as PbClBr is choose below: FW PbClBr / 6 x FW CoCBr6·H20 FW CoCBr6·H20 / FW PbClBr FW CoCBr6·H20 / 6 x FW PbClBr 6 x FW PbClBr / FW CoCBr6·H20
- A scientist wishes to measure the concentration of methyl benzoate in a plant stream by gas chromatography. He prepares a sample of butyl benzoate to use as an internal standard. The results of a preliminary run, which used a solution known to contain 1.37 mg/mL of methyl benzoate (peak A) and 1.51 mg/mL of butyl benzoate (peak B), are shown. The area of peak A is determined to be 3.40×102 and the area of peak B is determined to be 398 measured in arbitrary units by the computer. To measure the sample, 1.00 mL of a standard sample of butyl benzoate containing 2.49 mg/mL is mixed with 1.00 mL of the plant stream material. Analysis of the mixture gave a peak area of 437 for peak A and 415 for peak B. What is the concentration of methyl benzoate in the plant stream?if a volumetric pipet delivers 24.844g of deionized water at 31.00 degrees C, what is the calibrated volume of the pipet?How would you prepare 75 mL of an H2SO4 solution at 20% in weight (density=1.1394 g/mL, richness=227.9 g/L) starting from the commercial H2SO4 solution (98%, density=1.8361 g/mL, richness=1799 g/L)? Please choose among the most appropriate procedure which better describes the preparation of the previous diluted H2SO4 solution: Select one or more: a. Take the required volume of commercial H2SO4 solution with an adequate pipette, pour it into a graduated flask and add water up to the final volume (75 mL in this case). Homogenize the flask by stirring it gently. b. Take a beaker and put about 40 mL of distilled water. Then take the required volume of commercial H2SO4 solution with an adequate pipette and pour them over the beaker. Let the solution be warm and pour the mixture into a graduated flask and add water up to the final volume (75 mL in this case). Homogenize the flask by stirring it gently. c. Take a beaker and put about 40 mL of distilled water. Then take the required volume…
- 50 mg of granular salt is briefly stirred into a glass container of 1/5 liter volume filled with water. After briefly mixing, some salt is still seen at the bottom of the class. The visible salt is filtered from the water, weighed and determined to have a mass of 20 mg. What is the dissolved phase concentration of salt remaining in the water? Provide your answer to the nearest whole number in units of mg/l.1. The entire mercury bulb of the thermometer must be below the level of the side arm in order to obtain an accurate reading of the distillation temperature. Why is this so?2. Why is cold water circulated through the condenser from the bottom rather than from the top?4. In most distillations, the total volume of liquid obtained (distillate + residue) is not equal to the volume of the mixture introduced into the flask. What are the possible sources of loss in this procedure?A standard solution mixture containing each element at 500 ppm is provided. You will need to carefully dilute this so that your total volume is up to 50ml per standard solution mixture in the digitubes. Prepare calculations to show how you are going to prepare your calibration standards.
- (This question and the next 2 questions are breakdowns of the same question) A student John wanted to measure the molar mass of an unknown material (UM) via the boiling point change of a solvent. He chose a solvent, ethanol, that can dissolve the material and sugar. He wanted to use sugar (MW = 342.3 g/mol) as a reference sample to get an ebullioscopic constant for his system to reduce the effect of other measuring errors such as pressure, measuring errors, and impurity of the samples. He made 10 solutions each contain 100 g of ethanol and various amont of solute as list in the table. He fits the two sets of data and obtain the molar weight of the unknown materials. For this question answer the fitted boiling point of pure ethanol: ____ K. 4 sig. fig. Thre rest ? marks in the tale will be answered in the next two questions. Copy the data into Excel and use trendline to fit or calculate the average values for this and the next 2 questions. Sample # Sugar (g) B.P. (K) Sample # UM…What is the molarity of a concentrated solution of sulfuric acid with a specific gravity of 1.84 and 95.0% by weight sulfuric acid? specific gravity = density of substance at certain temp/density of water at 4 degrees C the density of water is 0.999973 g/mL at 4 degrees celsius. Describe how to prepare 3.0 L of 0.100M. I will pipet ______ and add this to 200mL water. The solution will be stirred and diluted to 3L with water.A pipet is used to transfer 6.00 mLmL of a 3.75 MM stock solution in flask “S” to a 25.00-mL volumetric flask “A,” which is then diluted with DI H2OH2O to the calibration mark. The solution is thoroughly mixed. Next, 10.00 mLmL of the solution in volumetric flask “A” is transferred by pipet to a 50.00-mL volumetric flask “B” and then diluted with DI H2OH2O to the calibration mark. Calculate the molarity of the solution in volumetric flask “B.”