a) Make a table of the chemical shift, multiplicity and number of hydrogens for each 1H-NMR signal. b) Propose a structure consistent with the data and assign each proton in your structure to a signal in the NMR spectrum.
a) Make a table of the chemical shift, multiplicity and number of hydrogens for each 1H-NMR signal. b) Propose a structure consistent with the data and assign each proton in your structure to a signal in the NMR spectrum.
Principles of Instrumental Analysis
7th Edition
ISBN:9781305577213
Author:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Chapter19: Nuclear Magnetic Resonance Spectroscopy
Section: Chapter Questions
Problem 19.12QAP
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Question
a) Make a table of the chemical shift, multiplicity and number of hydrogens for each 1H-NMR signal.
b) Propose a structure consistent with the data and assign each proton in your structure to a signal in the NMR spectrum.
Expert Solution
Step 1: Part a
Molecule is .
Divide each signal by lowest value of integration.
9.1 corresponds to
19.1 corresponds to
18.6 corresponds to
45.1 corresponds to
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