a) Make a table of the chemical shift, multiplicity and number of hydrogens for each 1H-NMR signal. b) Propose a structure consistent with the data and assign each proton in your structure to a signal in the NMR spectrum.

Principles of Instrumental Analysis
7th Edition
ISBN:9781305577213
Author:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Chapter19: Nuclear Magnetic Resonance Spectroscopy
Section: Chapter Questions
Problem 19.12QAP
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a) Make a table of the chemical shift, multiplicity and number of hydrogens for each 1H-NMR signal.

b) Propose a structure consistent with the data and assign each proton in your structure to a signal in the NMR spectrum.

Proton NMR
C3H100
8
1 ppm
6.
4
3.
45.1
Integration Values
18.6
19.1
9.1
Transcribed Image Text:Proton NMR C3H100 8 1 ppm 6. 4 3. 45.1 Integration Values 18.6 19.1 9.1
Expert Solution
Step 1: Part a

Molecule is C8H10O.

Divide each signal by lowest value of integration.

9.1 corresponds to 9.19.1=1

19.1 corresponds to 19.19.12

18.6 corresponds to 18.69.12

45.1 corresponds to 45.19.15

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