A Na,CO3 standard solution is prepared by transferring 2.4817 grams of primary standard-grade sodium carbonate to a 250.0 ml volumetric flask, dissolving the sample in -100 mL of distilled deionized water, and diluted to the mark. A 25.00 mL aliquot is taken and titrated with 42.65 mL of HCl solution to the bromocresol green endpoint. Calculate the concentration of the HCI solution. (А) 0.1598 M (В) 0.1098 М (©) 0.3196 M D) 0.05490 M
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- The total cation content of natural water is often determined by exchanging the cations for hydrogen ions on a strong acid ion-exchange resin. A 25.00 mL sample of a natural water was diluted to 100.00 ML with distilled water, and 2.06 g of a cation - exchange resin was added. After stirring, the mixture was filtered and the solid remaining on the filter paper was washed with three 15.00 mL portions of water. The filtrate and washings required 16.30 mL of 0.0282 M NaOH to give a bromocresol green end point. a) Calculate the number of millimoles of cation present in exactly 1.00 L of sample. b ) Report the results in terms of milligrams of CaCO3 per liter. Only typed solution.To determine the fluoride content in an aqueous and chloride-containing preparation of ammonium fluoride, the following analysis was performed. 105.2 mg of the preparation was dissolved in 100.0 mL of water. Then a 300 mL 40 mM lead chloride solution was added, whereby all fluoride ions were precipitated out of the solution in the form of the sparingly soluble salt PbClF (s). The precipitate was separated and washed at 15 degrees with a lead fluoride chloride saturated solution and dried at 130 degrees. The precipitate weighed 651.3 mg. a) Calculate the fluoride content (as % by weight F) in the preparation.b) Determine the purity of the ammonium fluoride preparationIn one trial determination of the concentration of NaOCl in the diluted bleach sample, 10.00 mL of the diluted bleach solution required 23.32 mL of 0.0195 M Na2S2O3 titrant to reach the endpoint. What is the molar concentration of NaOCl in the diluted bleach solution?
- a 10g soil sample was gently stirred with 250 ml of 1.0 M CH3COO(NH4) solution for 24 h and centrifuged to separate the solution. The solution recovered after centrifugation was titrated with distilled water to a volume of 1 liter and analyzed for cations. Analytical results showed that the solution contained 20 mg/L Ca, 2 mg/L Mg, 1 mg/L K, and 0.5 mg/L Na. Calculate the number of cation exchange equivalents and express it in meq/100 g of soilA Medical Technology student was given a capsule of a multivitamins and she was asked to determine the % by mass (w/w) of ascorbic acid present in the capsule. The student analyzed the 2.001 g sample using volumetric titration. The following data was generated in the analysis: KIO3 + 5KI + 6H+ → 3I2 + 6K+ + 3H2O C6H8O6 + I2 → C6H6O6 + 2I- + 2H+ Table 1. Standardization of KIO3 Molarity of Ascorbic Acid Standard Solution 0.03542 M Volume of Ascorbic Acid 25.00 mL Volume of KIO3 8.70 mL Molarity of KIO3 ______________M Table 2. Determination of Ascorbic Acid Concnetration Initial burette reading, KIO3 0.00 mL Final burette reading, KIO3 33.60 mL Volume consumed, KIO3 33.60 mL MM of Ascorbic Acid 176.12 g/mole choices 7.30% 30.1% 33.6% 32.5%The protein content of wheat flour can be determined reasonably accurately by multiplying the percentage of nitrogen present by 5.7. A 2.06-g sample of flour was taken through a Kjeldahl procedure and the ammonia produced was distilled into a boric acid solution. If this solution required 34.70 mL of 0.174 N HCl for titration to the methyl red end point, what is the a) % Nitrogen and b) % protein in the flour? (Use 1:1 stoich ratio between N and HCl)
- A commercial vinegar was analyzed by titration to determine the percent acetic acid. Briefly, 10.00 mL of vinegar sample was diluted to 100. mL solution in volumetric flask. A 25.00 mL aliquot from the diluted vinegar required 25.55 mL of 0.1005 M NaOH to reach the phenolphthalein endpoint. Which is the correct equation between the analyte and titrant reaction? CH3COOH + NaOH → NaCH3COO + H2O 2CH3COOH + NaOH → NaCH3COO + H2O C20H14O4 + NaOH → NaC20H14O4 + H2O CH3COOH + 2NaOH → NaCH3COO + H2OThe concentration of Cl– in a 300.0-mL sample of water drawn from a fresh water acquifer suffering from encroachment of sea water, was determined by titrating with 0.0516 M Hg(NO3)2. The sample was acidified and titrated to the diphenylcarbazone end point, requiring 6.18 mL of the titrant. Report the concentration of Cl–in parts per millionA saturated solution of magnesium hydroxide is prepared and the excess solid magneisum hydorixed is allowed to settle. A 25.0 mL aliquot of the saturated solution is withdrawn and transfered to a flask, two drops of inficator are added. A 0.00053 M HCL is dispensed from a buret into a solution. The solution changes color after the addition of 13.2 mL. What is the Ksp of magnesium hydroxide?
- To determine the concentration of glucose in the packaged juice industry, 50 mL of sample is analyzed. Analysis of it (and other reducing sugars) was carried out there using triiodide back titration. An excess volume of 75.00 mL of 0.338 M triiodide standard solution in alkaline medium was added to the glucose solution. The resulting solution was acidified and the excess triiodide was titrated with 18.37 mL of standard 0.526 M thiosulfate solution. Calculate is the concentration in ppm in the sample. In alkaline medium: Glucose (C6H12O6) / Gluconate (C6H11O7-), Triiodide (I3- ) / Iodide (I-) In acid medium: Thiosulfate (S2O32-) / Tetrathionate (S4O62-), Triiodide (I3- ) / Iodide (I-)describe how you can prepare 500mL of 0.10 M Fe2O3 (159.69g/mol) from the primary-standard-grade solid.Zhongli is a speleologist tasked to analyze the CaCO₃ content of a limestone stalactite. A 5.0000-g sample was dissolved in 25.00 mL of 1.350 M HCl, it was then heated to expel any CO₂ formed. The excess HCl was titrated to a phenolphthalein end point, it used 37.50 mL of 0.1200 M NaOH. How many moles of HCl was added initially to digest the limestone sample? How many moles of CaCO₃ is present in the limestone sample? What is the purity of the limestone in terms of %w/w CaCO₃?