a. Dotermine the callbration sensitivity of the method. b. Determine the exact LOD (in mg/L) for the method. c. Determine the exact LOQ (in mg/L) for the method.

Appl Of Ms Excel In Analytical Chemistry
2nd Edition
ISBN:9781285686691
Author:Crouch
Publisher:Crouch
Chapter15: Electrophoresis And Other Separation Methods
Section: Chapter Questions
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Chemistry
1. The foilowing calibration data were obtained by visible spectroscopy for the determination of FD&C
Yellow 5 in various food products:
Concentration of Standard
FD&C Yellow 5 (mg/L)
0.00
Number of replicate
measurements (n)
Mean analytical signal
(Abs)
0.099
Standard deviation
(Abs)
0.0081
0.0050
0.0080
0.0078
15
5.00
10
10.00
0.185
0.282
4.
15.00
4.
0.345
20.00
25.00
4
0.425
0.0085
0.0109
4
0.483
a. Determine the calibration sensitivity of the method.
b. Determine the exact LOD (in mg/L) for the method.
c. Determine the exact LOQ (in mg/L) for the method.
Transcribed Image Text:1. The foilowing calibration data were obtained by visible spectroscopy for the determination of FD&C Yellow 5 in various food products: Concentration of Standard FD&C Yellow 5 (mg/L) 0.00 Number of replicate measurements (n) Mean analytical signal (Abs) 0.099 Standard deviation (Abs) 0.0081 0.0050 0.0080 0.0078 15 5.00 10 10.00 0.185 0.282 4. 15.00 4. 0.345 20.00 25.00 4 0.425 0.0085 0.0109 4 0.483 a. Determine the calibration sensitivity of the method. b. Determine the exact LOD (in mg/L) for the method. c. Determine the exact LOQ (in mg/L) for the method.
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