Determine the identity of the solid organic compound in NMR spectra.  Include which protons cause the peaks in the H1 NMR and which carbons cause the peaks in C13 NMR. The list of all the possible organic compounds are as follows: Cumene, 3-Methy-2-butanone, Phenethyl alcohol, Isopropyl Acetate, Ethel benzoate, 3-phenylpropionaldehyde, isobutyl cinnamate, cyclamen aldehyde, Styrallyl acetate, Butyl butyrate, propiophenon, phenylacetylene, Cis-Hexenyl-3-Acetate, Benzyl propionate, 3-(p-ethyl-phenyl)-2,2-dimethyl propionaldehyde, 2-methoxy-4-ethyl-phenol, P-ethylphenol, diphenyl amine, 4-phenyl-3-buten-2-one, Diethyl Terphthalate, glutaric acid, cinnamic acid, P- ethylbenzoic acid, Coumarin, vanillin, (2,2,2-trichloro-1-phenylethyl)acetate, 4-(p-hydroxyphenyl)-2-butanone, 2-ethoxy-5-prop-1-enylphenol, t-butyl-phenol, Thymol, Calone, Syringol, Syringaldehyde.

Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
icon
Related questions
Question

Determine the identity of the solid organic compound in NMR spectra. 
Include which protons cause the peaks in the H1 NMR and which carbons cause the peaks in C13 NMR.

The list of all the possible organic compounds are as follows: Cumene, 3-Methy-2-butanone, Phenethyl alcohol, Isopropyl Acetate, Ethel benzoate, 3-phenylpropionaldehyde, isobutyl cinnamate, cyclamen aldehyde, Styrallyl acetate, Butyl butyrate, propiophenon, phenylacetylene, Cis-Hexenyl-3-Acetate, Benzyl propionate, 3-(p-ethyl-phenyl)-2,2-dimethyl propionaldehyde, 2-methoxy-4-ethyl-phenol, P-ethylphenol, diphenyl amine, 4-phenyl-3-buten-2-one, Diethyl Terphthalate, glutaric acid, cinnamic acid, P- ethylbenzoic acid, Coumarin, vanillin, (2,2,2-trichloro-1-phenylethyl)acetate, 4-(p-hydroxyphenyl)-2-butanone, 2-ethoxy-5-prop-1-enylphenol, t-butyl-phenol, Thymol, Calone, Syringol, Syringaldehyde. Borderline MP unknowns: Styrallyl alcohol, 1,1-dimethyl-2-phenethyl acetate, 1,1-dimethyl-2-phenyl ethanol.

Note: Mass of solid unknown sample added =0.050g and NMR Solvent(deuterated choloroform w/ 1% TMS)= 0.6ml 

9
F1: 60.201
EX: c:\left\HI\ACQ.ppg
7.804
992
8
7.553
7.497
7.438
7.355
7.281
7.245
7
7.115
6.483
6.326
SWI: 1000
PW: 14.4 us
6
5
PD: 3.0 sec
4
OF1: 360.3
NA: 1
3
LB: 0.0
2
PTS1d: 8192
000 0-
0 PPM
USER: DATE: 01/18/24 (17:17)
1
Transcribed Image Text:9 F1: 60.201 EX: c:\left\HI\ACQ.ppg 7.804 992 8 7.553 7.497 7.438 7.355 7.281 7.245 7 7.115 6.483 6.326 SWI: 1000 PW: 14.4 us 6 5 PD: 3.0 sec 4 OF1: 360.3 NA: 1 3 LB: 0.0 2 PTS1d: 8192 000 0- 0 PPM USER: DATE: 01/18/24 (17:17) 1
Expert Solution
trending now

Trending now

This is a popular solution!

steps

Step by step

Solved in 6 steps with 3 images

Blurred answer
Knowledge Booster
Nuclear Magnetic Resonance
Learn more about
Need a deep-dive on the concept behind this application? Look no further. Learn more about this topic, chemistry and related others by exploring similar questions and additional content below.
Similar questions
Recommended textbooks for you
Chemistry
Chemistry
Chemistry
ISBN:
9781305957404
Author:
Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:
Cengage Learning
Chemistry
Chemistry
Chemistry
ISBN:
9781259911156
Author:
Raymond Chang Dr., Jason Overby Professor
Publisher:
McGraw-Hill Education
Principles of Instrumental Analysis
Principles of Instrumental Analysis
Chemistry
ISBN:
9781305577213
Author:
Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:
Cengage Learning
Organic Chemistry
Organic Chemistry
Chemistry
ISBN:
9780078021558
Author:
Janice Gorzynski Smith Dr.
Publisher:
McGraw-Hill Education
Chemistry: Principles and Reactions
Chemistry: Principles and Reactions
Chemistry
ISBN:
9781305079373
Author:
William L. Masterton, Cecile N. Hurley
Publisher:
Cengage Learning
Elementary Principles of Chemical Processes, Bind…
Elementary Principles of Chemical Processes, Bind…
Chemistry
ISBN:
9781118431221
Author:
Richard M. Felder, Ronald W. Rousseau, Lisa G. Bullard
Publisher:
WILEY