DOW momorpo IR Spectrum (KBr disc) 1658 2000 4000 100 80 20 % of base peak 3284 3000 40 13C NMR Spectrum (50.0 MHz, CDCI, solution) 10 106 MIRE 137 80 120 160 200 m/e DEPT CH CH CH proton decoupled 200 ¹H NMR Spectrum (200 MHz, CDCI, solution) exchanges with D₂O on warming v (cm¹) 1600 160 if M** 179 120 expansion 1200 7.6 800 Mass Spectrum C10H13 NO₂ 240 280 solvent 80 7.0 ppm UV Spectrum Amax 250 nm (log, 3.1) Amax 287 nm (log, 2.2) solvent: chloroform 40 0 8 (ppm) TMS
DOW momorpo IR Spectrum (KBr disc) 1658 2000 4000 100 80 20 % of base peak 3284 3000 40 13C NMR Spectrum (50.0 MHz, CDCI, solution) 10 106 MIRE 137 80 120 160 200 m/e DEPT CH CH CH proton decoupled 200 ¹H NMR Spectrum (200 MHz, CDCI, solution) exchanges with D₂O on warming v (cm¹) 1600 160 if M** 179 120 expansion 1200 7.6 800 Mass Spectrum C10H13 NO₂ 240 280 solvent 80 7.0 ppm UV Spectrum Amax 250 nm (log, 3.1) Amax 287 nm (log, 2.2) solvent: chloroform 40 0 8 (ppm) TMS
Chapter13: Structure Determination: Nuclear Magnetic Resonance Spectroscopy
Section13.SE: Something Extra
Problem 59GP: The mass spectrum and 13C NMR spectrum of a hydrocarbon are shown. Propose a structure for this...
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From the MS data shown below, identify the unknown organic molecule. Indicate any partial structures that you are able to deduce from these spectra and explain how you identify these.
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