Draw and label a complete laboratory set-up of acid-base titration using phenolphthalein as the indicator, using HCl as the analyte/sample, and using NaOH as the standard solution. Cite complete source/(s) if picture will be copied from the internet.
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- A sample is known to contain about 20% soda ash. What sample size should be taken for analysis, if it is to be dissolved into a 50 mL volumetric flask, with 10 mL aliquots analyzed, if it is desired that the analysis consume a total of 40 mL 0.10 M HCl with 10 mL of 0.10 M NaOH used in the back-titration, after boiling.In the procedure below for a weak diprotic acid titation experiment what are the independent, dependent, and controlled variables? Prepare your Buret• Condition a 50 mL buret (2x with DI H2O followed by 2x standardized NaOH)• Fill the buret with the standardized NaOH close to but not exactly 0.00 mL Prepare Your Analyte • Your analyte will need to be placed in a 250 mL beaker and should contain thefollowing:*0.5 – 0.75 g KHP** About 100 mL DI water* Magnetic stir bar• Once all contents are in the 250 mL beaker, stir for at least 5 minutes to dissolve. Ifneeded, add a bit more water.* For unknown diprotic acids, use the mass provided by the instructorNext Run the Titration (note you will need to run the titration several times for data collection so you are able to use the average molar mass to find the unknown diaprotic acid).for the following, please identify the titrant and analyte!!! Prepare a titration for a 5mL borax solution, with a 0.52M HCl solution, sampled at 55 degrees Celsius.
- Which of the following steps MUST be done prior to titration of an analyte? I. Prepare a standardized solution II. Wash the burette with a standardized solution III. Fill the burette to the 50-mL mark IV. Prepare a contrast paper to determine burette volume and titration endpointCalculate the volume in liters of 0.545 M KOH necessary to titrate 0.0113 moles of hydrochloric acid, HCl, to a phenolphthalein end-point. Report the answer with three significant figures.An approximately 0.1-molar solution of NaOH is to be standardized by titration. Assume that the following materials are available. Clean, dry 50 mL buret •Analytical balance 250 mL Erlenmeyer flask •Wash bottle filled with distilled water Phenolphthalein indicator solution Potassium hydrogen phthalate, KHP, a solid monoprotic acid (to be used as the primary standard) Briefly describe the steps you would take, using the materials listed above, to standardize the NaOH solution. Describe (the set up) the calculations necessary to determine the concentration of the NaOH solution.
- A suitable target for the titration is 30.0 cm3 of 0.025 moldm-3 Br2(aq) Justify why a much smaller target titre would not be appropriate Calculate the amount in moles of bromine in the target titer Justification? calculate a suitable massof alive oil to transfer to the volumetric flask using your answer to of above question and the structure of Y Assume that the olive oil contains 85/- of Y by mass (If you were unable to calculate the amount of bromine in the target titer,you should assume it is 6.25×10^-8 mol .this in not the correct amount)why is it necessary to test the ph? EXTRME DETAIL PLEASE PROCEDURE To a six inch test tube was added thiamine hydrochloride (0.65 g), followed by water (2mL). The mixture was gently shaken until homogeneous, and then ethanol (7.5 mL)was added. Finally, sodium hydroxide (10%, 1.5 mL) was added and the mixture wasgently stirred to ensure complete mixing.Benzaldehyde (3.8 mL) was then added at room temperature in one portion with gentlestirring. The pH of the resulting reaction mixture was determined and adjusted to >10by dropwise addition of 10% sodium hydroxide.What conditions must be followed to perform complexometric titration?
- Which one of the following is NOT a source of error during a titration? Group of answer choices Adding too much sodium hydroxide solution to the analyte Refilling the buret during a titration trial Rinsing the buret with the analyte Adding indicator to the analyteWhy do you have to titrate until or above pH = 12.5 ± 0.2 to properly identify the unknown acid solution?Please answer with complete solutions. Do not use spreadsheet. Thank you A series of solutions containing NaOH, Na2CO3, and NaHCO3, alone or in compatible combination, was titrated with 0.1202 M HCl. Tabulated below are the volumes of acid needed to titrate 25.00-mL portions of each solution to (1) a phenolphthalein and (2) a bromocresol green end point. Use this information to deduce the composition of the solutions. In addition, calculate them molar concentration. (1) Phenolphthalein End Point (2) Bromocresol Green End Point a 22.42 22.44 b 15.67 42.13 c 29.64 36.42 d 16.12 32.23 e 0.00 33.33