Just want to make sure i am drawing the corret starting material before i submit. In this lab exercise would it be the hex-1-ene? Synthesis of Alcohols by Hydrating an AlkeneRefer to Lesson 35 for background information and the procedure to complete the prelab on Mastering ChemistryProcedurePart A. Synthesis of Hexan-2-ol.This part of the experiment must be done in the hood.1. Make an ice bath in a 250 mL beaker.2. Cool 15 mL of distilled water in a boiling tube provided by your instructor.3. Measure out 5 mL of hex-1-ene using a measuring a 10-mL graduated cylinder and pour it into another boilingtube. Cover the mouth of the tube with a wool.4.Cool the hex-1-ene in the ice bath for about three minutes.5. Measure out 5 mL of 75% sulfuric acid into another measuring cylinder.6.Remove the wool from the Boling tube. Slowly add the acid to the hex-1-ene, keeping the tube in the ice bathand stirring the mixture with a glass rod. ADDING LARGE AMOUNTS OF THE ACID MAY CAUSE EXPLOSION!7. When all the acid has been added, continue to stir the mixture until ONLY ONE LAYER IS OBSERVED. This willtake about 5-10 minutes. Cover the boiling tube with the wool.8.Allow the mixture to stand in the ice bath for another 5 minutes, then carefully add an equal volume of colddistilled water from the other boiling tube. The mixture should separate into two layers. The top layer containsthe product, the lower layer contains mainly sulfuric acid solution.Part B. Separation and Washing the Product1. Transfer the contents of the boiling tube from step 8 into a 50-mL beaker, and then pour the reaction mixtureinto a small separating funnel, stopper, shake and allow the contents to settle.2. Open the stopcock to run off the lower layer into another 50-ml beaker.3. Wash the product by adding 10 mL distilled water to the separating funnel, stopper and shake. Remove thelower layer.4.Place 25 g of anhydrous sodium carbonate in a 50-mL or 100-mL Erlenmeyer flask.5. Run off the product of the separating funnel into the Erlenmeyer flask. Swirl the flask frequently for twentyminutes to dry the product.Part C. Distillation of the product1. Set up a simple distillation apparatus.2. Decant as much as possible the product from the Erlenmeyer flask into the distilling flask (25-mL or 50-mL round Draw the structure of the starting material in this hydration experiment.H: 2D EXP CONT: 1NNMarvin JSby ChemAxonC[1]ASwwwmaHсz ONSにBr-PLLF

This experiment is synthesis of hexan-1-ol by hydration of hex-1-ene.

Answered: Draw the structure of the starting…

Science

Chemistry

Draw the structure of the starting material in this hydration experiment.

Organic Chemistry: A Guided Inquiry

2nd Edition

ISBN:9780618974122

Author:Andrei Straumanis

Publisher:Andrei Straumanis

Chapter13: Substitution

Section: Chapter Questions

Problem 2E

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Please answer the question at the bottom, Thanks. LAB NOTES FOR PREPARATION OF BUTYL MAGNESIUM BROMIDEAND ITS SUBSEQUENT CONVERSION TO AN ALCOHOL To the reaction flask were added 2.5967 gram of magnesium turnings, about 20 mlof diglyme, and a solution of 13.5942 gram of butyl bromide in about 25 mldiglyme.The procedure as per the lab manual was initiated. After the required heating timewas completed the reaction mixture was allowed to cool to room temperature.Then a solution of 6.1123 gram of acetone in about 15 ml of diglyme was addeddropwise as per the lab manual.The rest of the lab manual procedure was completed, ultimately affording 2.5532gram of an oily, clear and slightly yellow liquid, presumed to be 2-methyl-2-hexanol. Boiling point as measured by distillation was 138 – 141 deg C.About 0.8 ml of the presumed 2-methyl-2-hexanol was placed in an NMR tube towhich was added 2 drops of TMS. The tube was capped, then inverted and righted20 times to thoroughly mix the product and…
Please answer the question at the bottom, Thanks. LAB NOTES FOR PREPARATION OF BUTYL MAGNESIUM BROMIDEAND ITS SUBSEQUENT CONVERSION TO AN ALCOHOL To the reaction flask were added 2.5967 gram of magnesium turnings, about 20 mlof diglyme, and a solution of 13.5942 gram of butyl bromide in about 25 mldiglyme.The procedure as per the lab manual was initiated. After the required heating timewas completed the reaction mixture was allowed to cool to room temperature.Then a solution of 6.1123 gram of acetone in about 15 ml of diglyme was addeddropwise as per the lab manual.The rest of the lab manual procedure was completed, ultimately affording 2.5532gram of an oily, clear and slightly yellow liquid, presumed to be 2-methyl-2-hexanol. Boiling point as measured by distillation was 138 – 141 deg C.About 0.8 ml of the presumed 2-methyl-2-hexanol was placed in an NMR tube towhich was added 2 drops of TMS. The tube was capped, then inverted and righted20 times to thoroughly mix the product and…
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