Having too much sample can cause an inaccurate melting point under these Sir how will the observed melting point compare with the true melting point ?

Macroscale and Microscale Organic Experiments
7th Edition
ISBN:9781305577190
Author:Kenneth L. Williamson, Katherine M. Masters
Publisher:Kenneth L. Williamson, Katherine M. Masters
Chapter3: Melting Points And Boiling Points
Section: Chapter Questions
Problem 9Q: You have an unknown with an observed melting point of 90C-93C. Is your unknown compound A with a...
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Having too much sample can cause an inaccurate melting point under these Sir how will the observed melting point compare with the true melting point ?

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If heating occurs too quickly, the material cannot reach thermal equilibrium. Pure substances melt over a short range of temperature (usually over a few degrees).

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