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Identify the structure of the important fragments. Show the arrow pushing mechanism to form the significant fragments. Suggest possible structure based on MS and IR data.

Identify the structure of the important fragments. Show the arrow pushing mechanism to form the significant fragments. Suggest possible structure based on MS and IR data.

Organic Chemistry
Organic Chemistry
8th Edition
ISBN:9781305580350
Author:William H. Brown, Brent L. Iverson, Eric Anslyn, Christopher S. Foote
Publisher:William H. Brown, Brent L. Iverson, Eric Anslyn, Christopher S. Foote
Chapter14: Mass Spectrometry
Section: Chapter Questions
Problem 14.37P
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Identify the structure of the important fragments. Show the arrow pushing mechanism to form the significant fragments. Suggest possible structure based on MS and IR data. 2. MF C₂H₂O IR KBr Disc LOD 2000 1500 1000 500 HAVENUMBERI MANSHYTANLETE 8 4000 3132 77 3322 79 3065 86 3040 70 3029 68 2992 74 2014 09 3000 2744 64 2716 74 1677 4 1627 14 1606 49 1597 55 1676 47 1496 68 1450 34 1395 74 1329 74 1306 66 1295 52 1262 62 55 1204 74 1179 66 1150 1126 1073 58 1008 52 973 27 6 646 79 748 19 25 620 74 606 50 584 49 601 64 609
Transcribed Image Text:Identify the structure of the important fragments. Show the arrow pushing mechanism to form the significant fragments. Suggest possible structure based on MS and IR data. 2. MF C₂H₂O IR KBr Disc LOD 2000 1500 1000 500 HAVENUMBERI MANSHYTANLETE 8 4000 3132 77 3322 79 3065 86 3040 70 3029 68 2992 74 2014 09 3000 2744 64 2716 74 1677 4 1627 14 1606 49 1597 55 1676 47 1496 68 1450 34 1395 74 1329 74 1306 66 1295 52 1262 62 55 1204 74 1179 66 1150 1126 1073 58 1008 52 973 27 6 646 79 748 19 25 620 74 606 50 584 49 601 64 609
Identify the structure of the important fragments. Show the arrow pushing mechanism to form the significant fragments. Suggest possible structure based on MS and IR data. 2. MF C₂H₂O 131(Base peak 27.0 1.5 28.0 100 1.1 29.0 1.0 38.0 1.2 39.0 3.7 50.0 8.6 51.0 21.2 80 51.5 1.1 52.0 5.5 53.0 1.2 54.0 1.0 55.0 1.1 61.0 1.1 62.0 2.5 63.0 5.7 1.1 65.0 74.0 5.3 75.0 4.7 77 76.0 5.1 77.0 35.7 78.0 26.1 79.0 1.7 51 89.0 1.2 91.0 2.5 101.0 1.5 102.0 8.9 103.0 54.5 104.0 27.4 105.0 3.5 131.0 100.0 132.0 74.8 133.0 7.3 Relative Intensity 40 20 O qoympt|t|ypt 25 50 75 m/z m 103 100 125 132(M+) 133(M+1) 150
Transcribed Image Text:Identify the structure of the important fragments. Show the arrow pushing mechanism to form the significant fragments. Suggest possible structure based on MS and IR data. 2. MF C₂H₂O 131(Base peak 27.0 1.5 28.0 100 1.1 29.0 1.0 38.0 1.2 39.0 3.7 50.0 8.6 51.0 21.2 80 51.5 1.1 52.0 5.5 53.0 1.2 54.0 1.0 55.0 1.1 61.0 1.1 62.0 2.5 63.0 5.7 1.1 65.0 74.0 5.3 75.0 4.7 77 76.0 5.1 77.0 35.7 78.0 26.1 79.0 1.7 51 89.0 1.2 91.0 2.5 101.0 1.5 102.0 8.9 103.0 54.5 104.0 27.4 105.0 3.5 131.0 100.0 132.0 74.8 133.0 7.3 Relative Intensity 40 20 O qoympt|t|ypt 25 50 75 m/z m 103 100 125 132(M+) 133(M+1) 150
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