IRil. 4 Stretch NaOH (aq) + 2 H2O 58.05 t84.79 g/me| :a 5 mL round-bottom-flask (RBF) equipped with magnetic stirring bar place 4.0 mL c solution, and add 3.2 mL of 95 % ethanol, 40 mL of benzaldehyde. Finallý add 0.15

Organic Chemistry
8th Edition
ISBN:9781305580350
Author:William H. Brown, Brent L. Iverson, Eric Anslyn, Christopher S. Foote
Publisher:William H. Brown, Brent L. Iverson, Eric Anslyn, Christopher S. Foote
Chapter19: Enolate Anions And Enamines
Section: Chapter Questions
Problem 19.55P
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I need help predcting the 1hnmr of the product and give the chemical shift and mutiplcity of for each proton 

1 ilearn.laccd.edu/courses/188213/pages/synthesis-of-dibenzalacetone-1-5-diphenyl-1-4-pentadien-3-one-by-mixed-aldol-condensation?module_item_id... Q O *
* M
Update
Stuetch
NaOH (aq)
+ 2 H20
58.09
284.19 9/mol
re:
25 mL round-bottom-flask (RBF) equipped with magnetic stirring bar place 4.0 mL c
solution, and add 3.2 mL of 95 % ethanol, 40 mL of benzaldehyde. Finallý add 0.15
ction mixture. Cap the RBF and mix the reaction mixture continuonsly for 30 minute
Transcribed Image Text:1 ilearn.laccd.edu/courses/188213/pages/synthesis-of-dibenzalacetone-1-5-diphenyl-1-4-pentadien-3-one-by-mixed-aldol-condensation?module_item_id... Q O * * M Update Stuetch NaOH (aq) + 2 H20 58.09 284.19 9/mol re: 25 mL round-bottom-flask (RBF) equipped with magnetic stirring bar place 4.0 mL c solution, and add 3.2 mL of 95 % ethanol, 40 mL of benzaldehyde. Finallý add 0.15 ction mixture. Cap the RBF and mix the reaction mixture continuonsly for 30 minute
Synthesis of Dibenzalacetone (1,5-Diphenyl-1A-pentadien-3-one)
By Mixed-Aldol Condensation
General Equation:
CHO
NaOH (aq)
+ 2 H20
58.05
r84. 79 g/mo)
General Procedure:
Into a clean 25 mL round-bottom-flask (RBF) equipped with magnetic stirring bar place 4.0 mL of 10
% sodium hydroxide solution, and add 3.2 mL of 95 % ethanol, 40 mL of benzaldehyde. Finallý add 0.15 mL
of acetone to the reaction mixture. Cap the RBF and mix the reaction mixture continuously for 30 minutes. If
no solid product forms, open the container and scratch inside the RBF, under the liquid with a glass rod. After
30 minutes, remove the liquid from the vial using a Pasteur pipette by squeezing the bulb of the pipette,
pressing the pipette tip flat against the bottom of the vial, and bringing the liquid up while leaving the crystals
Transcribed Image Text:Synthesis of Dibenzalacetone (1,5-Diphenyl-1A-pentadien-3-one) By Mixed-Aldol Condensation General Equation: CHO NaOH (aq) + 2 H20 58.05 r84. 79 g/mo) General Procedure: Into a clean 25 mL round-bottom-flask (RBF) equipped with magnetic stirring bar place 4.0 mL of 10 % sodium hydroxide solution, and add 3.2 mL of 95 % ethanol, 40 mL of benzaldehyde. Finallý add 0.15 mL of acetone to the reaction mixture. Cap the RBF and mix the reaction mixture continuously for 30 minutes. If no solid product forms, open the container and scratch inside the RBF, under the liquid with a glass rod. After 30 minutes, remove the liquid from the vial using a Pasteur pipette by squeezing the bulb of the pipette, pressing the pipette tip flat against the bottom of the vial, and bringing the liquid up while leaving the crystals
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