mass. 0.55g 136.159 Methylbenzoate pooduces 181.139 nito Pat. 0:55g 181.13 x0:55g 136-15 Theoretical yield 0.7317g Nitration of Acetanilide NO2 | 35-17glnol 160.16g Im1 0.5g mass: Acetanilide produre I Boi169 Paodic * 135.179 1 80.16 X0.59 .0:59 " :0.59 135.17 Theaeticalyield 0.66649 theoretical yieds were Calculated.

Fundamentals Of Analytical Chemistry
9th Edition
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Author:Skoog
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Chapter7: Statistical Data Treatment And Evaluation
Section: Chapter Questions
Problem 7.9QAP
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Nitration of methyl benzoate:

Weight of filler paper: 0.682g

Mp product: 76-77 C

Nitration of Acetanilide:

Weight of filler paper: 0.691g

Weight of filler paper product: 1.232g

Mp product: 212-214 C

Compound

MM (g/mol)

ortho mp (oC)

meta mp (oC)

para mp (oC)

Nitroacetanilide

180.16

94

155

214-217

Methyl nitrobenzoate

181.15

-13

78-80

94-96

Theoretical yield of acetanilde: 0.6664g 

Theoretical yield of methyl benzoate: 0.7317g

  • find theoretical yield of methyl nitrobenzoate                                              percent yield of your methyl nitrobenzoate and melting point of your methyl nitrobenzoate
Reagents and Properties
afni
molar mass
substance
quantity
(g/mol)
d (g/mL)
mp (C) bp ("C)
acetanilide
0.5 g
5-10 mL
135.17
113-115
ethanol, 95%
methyl benzoate
methyl
nitrobenzoate*
46.07
78
0.55 g
136.15
1.094
-12
198
181.13
DowA dos
bood amut
nitroacetanilide*
180.16
nitric acid conc.
0.5 mL
63.01
sulfuric acid conc. 1.6 mL
98.08
"product
od i odt "bi
Transcribed Image Text:Reagents and Properties afni molar mass substance quantity (g/mol) d (g/mL) mp (C) bp ("C) acetanilide 0.5 g 5-10 mL 135.17 113-115 ethanol, 95% methyl benzoate methyl nitrobenzoate* 46.07 78 0.55 g 136.15 1.094 -12 198 181.13 DowA dos bood amut nitroacetanilide* 180.16 nitric acid conc. 0.5 mL 63.01 sulfuric acid conc. 1.6 mL 98.08 "product od i odt "bi
Nitsation of Methylbenzoate
Por Nitratio
NO2
MD: 136-15glol
181.13 g/ml
mass:
0.55g
136-159
Methylbenzoate produces
Te1.139 nito
Pdt.
0:55g"
" 181.13
136-15
Theoretical yield 0.73179
Nitration of Acetanilide
[D]
135-17glnol
16016g lm1
mass:
135.179
Acetanilide produre Boo169 Paoduct
1 80.16 X0:59
135.17
Theeseticalyield0.66649
: theoretical yieds were calculated.
Transcribed Image Text:Nitsation of Methylbenzoate Por Nitratio NO2 MD: 136-15glol 181.13 g/ml mass: 0.55g 136-159 Methylbenzoate produces Te1.139 nito Pdt. 0:55g" " 181.13 136-15 Theoretical yield 0.73179 Nitration of Acetanilide [D] 135-17glnol 16016g lm1 mass: 135.179 Acetanilide produre Boo169 Paoduct 1 80.16 X0:59 135.17 Theeseticalyield0.66649 : theoretical yieds were calculated.
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Theoretical yield is the mathematically weight of the product .

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