O https://ovg.cengagenow.com/iln/t Draw the structure(s) of the major organic product(s) of the following reaction. Trace of acetic acid NH2 +] ethanol
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- Given this organic synthesis, is there any limiting and excess reagents? also describe the procedure is run, how is the reaction monitored?Is the order fo addition important? N-ETHYLALLENIMINE[Aziridine, 1-ethyl-2-methylene-] Submitted by Albert T. Bottini and Robert E. Olsen1.Checked by Thomas H. Lowry and E. J. Corey. 1. ProcedureCaution! This preparation should be carried out in a good hood to avoid exposure to ammonia. The operator should wear rubber gloves and protective goggles because 2-haloallylamines and ethylenimines can cause severe skin and eye irritation. A 2-l. three-necked flask is fitted with a sealed mechanical stirrer, a gas-inlet tube, and a dry ice condenser protected from the air by a soda-lime drying tube (Note 1). The system is flushed thoroughly with dry ammonia, and 32.8 g. (0.84 mole) of sodium amide (Note 2) is added to the flask. The system is again flushed with ammonia, the condenser is provided with dry ice covered by acetone, and 1.2 l. of liquid…I’m currently trying to write a lab report for the synthesis of dimolybdenum tetraacetate [Mo2(O2CCH3)4] from the reaction of molybdenum hexacarbonyl, Mo(CO)6 in glacial acetic acid and acetic anhydride under a nitrogen atmosphere, involving the difficult formation of a quadruple bond and requires high heat and long reaction time (approximately 20 hours). But these are the question I’m stumped on: 1. Why need the reaction be done under nitrogen? We also added dichlorobenzene and hexanes during the reaction. 2. Explain the purpose of dichlorobenzene and hexanes. 3. Why does the reaction take 20 hrs?During an acid base extraction of an organic compound dissolved in dichloromethane with sodium bicarbonate (NaHCO3), you do not recover any of the desired extracted product after completing all the remaining steps. What could the most probable reason(s) be for the observed outcome? -The organic compound you want to extract is also a base; an acid is needed -You did not degassed/vent the separatory funnel -You did not shake the separatory funnel enough to react the base with the organic compound -You did not heat the mixture before the extraction -The organic compound evaporate from separatory funnel during the extraction
- Tunicates are marine animals that are called "sea squirts" because when they are taken out of water, they tend to contract and expel seawater. Lepadiformine is a cytotoxic agent (toxic to cells) isolated from a marine tunicate. During a recent synthesis of lepadiformine, the investigators observed the formation of an interesting by-product (3) while treating diol 1 with a reagent similar in function to PBr3 (J. Org. Chem. 2012, 77, 3390–3400):In light of your answer to Problem 30-40, explain why a mixture of products occurs in the following reaction:How to approach and solve the problem, thank u
- ANSWER ASAP Please show the electron-flow mechanism of nitrobenzene to aniline. This involves predicting major and by-products using electronic and structural effects. The arrow push mechanism must be shown.Write out the reaction of Bromination of E-stilbene using chemdraw (ACS 1996 format). Include all reagents, products, solvents, reaction temperature and yield. Reagents used include glacial acetic acid, E-stilbene, and pyridinium perbromide, otherwise known as PHPB. Glacial acetic acid: 10mL Stilbene: 0.5g Perbromide: 1.0g Product yield (Precipitate) weight: 0.63g(ii) The elimination reaction between 2-bromobutane and NaOCH2CH3 gives two organic products. Draw a mechanism for the reaction which produces the major organic elimination product and provide a rationale as to why that is the major product.(with explanation)
- Give mechanism of norrish type 1 reaction of cyclopentanone in gas phase and in solution phase Please answer ASAPEnamines formed from the cyclic secondary amine pyrrolidine are important intermediates in the synthesis of 1,5-diketones. (1st pic) On the structures provided below, draw arrows showing electron flow for the reaction mechanism for the acetic acid-catalyzed formation of an enamine from cyclohexanone and pyrrolidine. (2nd pic)SHOW COMPLETE SOLUTIONS Q3. Which isolate has A260/280 ratio of above 2.0?