Organic Derivatives of water Solubility in H20 Solubility in NaOH Bayer's oxidation Chromic Lucas test Ferric acid oxidation chloride test Visible + result SAMPLES Ethanol 2-Butanol tert-Butanol ++ ++ ++ ++ ++ ++ Phenol Diethyl ether Unknown 1 Unknown 2 Unknown 3 Legend: ++> fast reaction/completely soluble; + > slow reaction/slightly soluble; - > no reaction/insoluble ++ ++ ++ + ++ Identities of Unknown Samples Sample 1: Sample 2. Sample 3. A. Pertinent General Reactions (1) Bayer's oxidation: (2) Chromic acid oxidation: (3) Lucas test (4) Ferric chloride test

Fundamentals Of Analytical Chemistry
9th Edition
ISBN:9781285640686
Author:Skoog
Publisher:Skoog
Chapter7: Statistical Data Treatment And Evaluation
Section: Chapter Questions
Problem 7.9QAP
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Organic Derivatives of water
Solubility
in H20
Solubility
in NaOH
Chromic
Вayer's
oxidation
Lucas test
Ferric
acid
oxidation
chloride
test
Visible +
result
SAMPLES
Ethanol
2-Butanol
tert-Butanol
Phenol
Diethyl ether
Unknown 1
Unknown 2
++
++
++
-
+
++
++
+
++
+
+
++
+
++
++
Unknown 3
Legend: ++ > fast reaction/completely soluble; + > slow reaction/slightly soluble; -> no reaction/insoluble
+
++
Identities of Unknown Samples
Sample 1:
Sample 2:
Sample 3:
A. Pertinent General Reactions
(1) Bayer's oxidation:
(2) Chromic acid oxidation:
(3) Lucas test
(4) Ferric chloride test
Transcribed Image Text:Organic Derivatives of water Solubility in H20 Solubility in NaOH Chromic Вayer's oxidation Lucas test Ferric acid oxidation chloride test Visible + result SAMPLES Ethanol 2-Butanol tert-Butanol Phenol Diethyl ether Unknown 1 Unknown 2 ++ ++ ++ - + ++ ++ + ++ + + ++ + ++ ++ Unknown 3 Legend: ++ > fast reaction/completely soluble; + > slow reaction/slightly soluble; -> no reaction/insoluble + ++ Identities of Unknown Samples Sample 1: Sample 2: Sample 3: A. Pertinent General Reactions (1) Bayer's oxidation: (2) Chromic acid oxidation: (3) Lucas test (4) Ferric chloride test
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