how do I find the yield with the characterization Product characterization:0.91 g of the crude product0.77 g of the final productМ.р. (crude): 85-93 °CМ.р. (final): 104-106 °C Setup:• placed 1.15 g of 1,4-dimethoxybenzene, 2.2 mL of tert.-butyl alcohol, and 3.4 mL glacialacetic acid in a 125-mL Erlenmeyer flask• the mixture was swirled until the solids dissolved and then placed in an ice bath for10 minutesRunning the reaction:• 4.50 mL of concentrated sulfuric acid were placed in an ice bath for 10 minutes• the sulfuric acid was added dropwise to the cooled reaction mixture while swirling(~ 10 minutes)• the reaction mixture was placed on the bench and allowed to warm up to room temperature(~15 minutes), was swirled three times during this timeProduct isolation:• 14 g of ice was added to the reaction mixture before 50 mL of water was added to causeprecipitation of a beige-colored solid• the solids were isolated on a small Büchner funnel using vacuum filtration, washed withwater, and allowed to dry until the next meeting• the crude product was recrystallized from a total of 10 mL of hot methanol• the solution could cool to room temperature (~10 minutes) and then placed in an ice bath(~15 minutes)• Upon cooling, a light beige solid formed that was isolated by vacuum filtration• The solid was washed with 2 mL of ice-cold methanol and then air sucked through thesolids to dry them (20 minutes)Product characterization:0.91 g of the crude product• 0.77 g of the final productМ.р. (сrude): 85-93 °CМ.р. (final): 104-106 °C

Given: Mass of Crude product = 0.77 g Mass of Final product = 0.91 g

Answered: Product characterization: 0.91 g of the…

Fundamentals Of Analytical Chemistry

9th Edition

ISBN:9781285640686

Author:Skoog

Publisher:Skoog

Chapter8: Sampling, Standardization, And Calibration

Section: Chapter Questions

Problem 8.1QAP

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Product characterization: 0.91 g of the crude product 0.77 g of the final product M.p. (crude): 85-93 °C • M.p. (final): 104-106 °C