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- please quickly thanks ! 3.Please write out the major reaction and side-reaction in the preparation of ter-butyl.chloride, and write out the key points to use separation funnel in this process.I am working on a practice assignment for my organic II course and am having difficulty with a question that asks to identify the reaction sequence used to synthesize isopropylcyclopentane. I would really appreciate the help!How do I report this data? Blue is background data, red is compound 1-bromo-3-phenylpropane, synthesized from 3-phenyl-1-propanol using Nabr and h2so4.
- Need help showing the reaction mechanism between LDA and 2-chloropyridine. Show all reaction steps and transition states. Also include interactions and brackets as well as show all products and byproducts. Thank you :)1. Draw a complete mechanism for the acid-catalyzed esterification of acetic acidwith ethanol. Then answer the follow-up questions:a) Every step in this reaction is an equilibrium. Comment on all of the possibleways to drive the equilibrium (there should be four ways.)b) If some carboxylic acid remains at the end of the reaction, what are somepossible ways to get rid of it?c) If excess alcohol remains at the end of the experiment, what are some possibleways to get rid of it?Calculate the theoretical yield of virstatin ethyl ester and virstatin. Procedure – Step 1 Synthesis of virstatin ethyl ester (with notes and musings about procedural steps in italics) 1,8-naphthalimide (0.25 g) and potassium carbonate (0.26g) are added to a 10 ml round bottom flask containing a stir bar. 1.3 ml DMF (N,N-dimethylformamide) is added to the flask. The DMF will be in a “sure seal” bottle with a septum. You will obtain the DMF using a syringe and needle. Wear gloves when obtaining and dispensing the DMF. Add ethyl 4-bromobutanoate (0.27 ml) (it might say ethyl 4-bromobutyrate on the bottle) to the reaction flask, using an automatic pipet. Heat under reflux, with stirring, for 1 hour. What will the sand temperature have to be to get DMF to boil?? When would you start heating the sand!? After cooling to room temperature add 5 ml water to the reaction solution and cool the resulting mixture in an ice bath. Using a Buchner funnel, vacuum filter the ice cold…
- How different would step 4 be if the amine was secondary? Show curved arrows and explain the mechanism!An organic chemistry experiment involves a nucleophilic substitution (SN2) reaction using 1-iodobutane and 2-naphthoxide ion. The 2-naphthoxide ion is generated from 2-naphthol and sodium hydroxide in an ethanol solvent. The experiment includes steps like generating the nucleophile, conducting the SN2 reaction, and analyzing the product using 1H NMR spectroscopy. Question: Write the structure of the undesired side product if CH3CH2O‾ (ethoxide) reacts with 1-iodobutane.Describe how the product is purified. 4,4'-DIBROMOBIPHENYL [Biphenyl, 4,4'-dibromo-] Submitted by Robert E. Buckles and Norris G. Wheeler1. Checked by R. S. Schreiber, Wm. Bradley Reid, Jr., and Robert W. Jackson. 1. Procedure In a 15-cm. evaporating dish is placed 15.4 g. (0.10 mole) of finely powdered biphenyl (Note 1). The dish is set on a porcelain rack in a 30-cm. desiccator with a 10-cm. evaporating dish under the rack containing 39 g. (12 ml., 0.24 mole) of bromine. The desiccator is closed, but a very small opening is provided for the escape of hydrogen bromide (Note 2). The biphenyl is left in contact with the bromine vapor for 8 hours (or overnight). The orange solid is then removed from the desiccator and allowed to stand in the air under a hood for at least 4 hours (Note 3). At this point, the product weighs about 30 g. and has a melting point in the neighborhood of 152°. The crude 4,4'-dibromobiphenyl is dissolved in 75 ml. of benzene, filtered, and cooled to 15°. The…
- Draw the product of the reactions of succinic anhydride with each of the listed reagents. Assume in all cases that the reagent is present in excess and an aqueous workup takes place after each reaction. A. Reaction with (CH3)2CHOH. \table[[Select,Draw,Templates More,,],[/,//,I//,H,Erase]] B. Reaction with NH3. \table[[Select,Draw,tes More,Erase],[/,//,III,C,H,N,0]] Question Source: Vollhardt 7e0 Organic Chemistry: Structure And Function Publishęr: W. Freemar C. Reaction with phenylmagnesium bromide in THF, followed by H+,H2o. \table[[Select,Drav,v T,lates,,,Erase],[1,II,III,C,H,0,]] D. Reaction with LiAlH4 in ether, followed by H+,H2O \table[[Select,Draw,Templates More],[/,//,III]] \table[[3,0]] \table[[,2,QA. Give a product that contains carboxylic acid found in the market. Name of product Carboxylic acid present and its uses B. Give a product that contains ester found in the market. Name of product Ester present and its uses I WILL UPVOTE BUT PLS BE INFORMATIVE, THANK YOUUUSelf-condensation of acetone is a possible side reaction for the aldol condensation(Reaction 1). Draw the structure of this side product. How is this side reaction minimizedin our procedure written below? Reaction 1 - Experimental Procedure: In a clean, small Erlenmeyer flask, combine your unknownaromatic aldehyde (350 μL (400 mg if it is a solid)), 95% ethanol (2.0 mL), and 5 N aqueoussodium hydroxide (0.6 mL). Swirl to mix, and then add acetone (100 μL). Stir/swirl vigorously for30 minutes, until precipitation is complete. If no precipitate forms after 15 minutes, heat theErlenmeyer flask gently in on the sand bath in the hood for 15 minutes, and then allow it to coolto room temperature. Whether heated or not, cool your Erlenmeyer flask in an ice bath for 10minutes to ensure complete crystallization. Collect the product by vacuum filtration. (If you donot have any solid at this point, evaporate all solvent in the sand bath. Recrystallize if solidresidue is obtained; otherwise stop…
