14 15 or this experiment, yield was not important, but in onsite lab, as well as large-scale processes, a good yield is crucial in the success of a purification step. In what ways doou think a high yield can be assured in recrystallization?BBIUA A LEX² X₂ EEE 12ptParagraphM2 frPreviousto searchEl3'L30°C Haze ENG5:48 pm23/05/2022NextOE A student ran a TLC plate using a 90:10 hexane:ethyl acetate developer and this was the outcome. How can they improve their next trial?15BIU AAI EE x²x, E 12ptParagraph-GBfrEtG230°C Haze GENGe here to search175:48 pm

this experiment, yield was not important, but in onsite lab, as well as large-scale processes, a good yield is crucial in the success of a purification step. In what ways do think a high yield can be assured in recrystallization?

this experiment, yield was not important, but in onsite lab, as well as large-scale processes, a good yield is crucial in the success of a purification step. In what ways do think a high yield can be assured in recrystallization?

Principles of Instrumental Analysis

7th Edition

ISBN:9781305577213

Author:Douglas A. Skoog, F. James Holler, Stanley R. Crouch

Publisher:Douglas A. Skoog, F. James Holler, Stanley R. Crouch

Chapter33: Automated Methods Of Analysis

Section: Chapter Questions

Problem 33.8QAP

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Make a schematic diagram for the procedure below: B. % SO3 determination Dry the soluble sulfate sample at 100° C for 1-2 hours, and cool in desiccator. Weigh out 0.5 – 0.7 g (± 0.3 mg) duplicates sample. Transfer to 400-mL beakers. Dissolve each in 200 mL of dist. H2O + 4 mL of 6 m HCl. Precipitant is prepared by dissolving 1.3 g BaCl2 ∙ H2O in 100 mL water. Filter if solution is not perfectly clear. Heat the BaCl2 solution and sulfate sample solution nearly to boiling, and then add the entire amount to the HOT sulfate sample solution while stirring vigorously. Wash stirring rod with distilled water and include washings in your final mixture. Digest by letting stand 1-2 hours. Overnight standing is acceptable. Filter through an ash less filter paper of fine porosity (Whatman no. 42). Slowly pour the supernatant liquid through the filter paper.
I just need help figuring out the values to do a calculation. Part of the lab relevant... "Prepare standards on the same day they will be used. Using a 100 mL volumetric flask, add x mL (vide infra) of the 0.050 mg/mL phosphate standard, 20 mL of th e molybdate-antimoney reagent, 1 mL of ascorbic acid, and dilute to volume with ultrapure water. Do this procedure for x = 0 mL, 1 ml, 2 ml, 5 ml, and 10 ml using volumetric pipettes. To be clear, we will be making 5 different solutions. The equation that was given was Concentration of initial standard (mg/mL) multiplied by volume added (mL) = concentration of created standard multiplied by volume of volumetric I dont need you to do the calculations, I just need help finding what values go in equation. we are trying to find the concentration of created standard
MAKE A METHODOLOGY : MATERIALS/ REAGENTS WITH SCHEMATIC DIAGRAM . THE PICTURE UPLOADED SERVES AS A GUIDE, DO THE SAME THING BASED FROM THE PIC. Procedure: Place 20 drops of each of 0.2M CuSO4 in a centrifuge tube. Then add 5 drops of freshly prepared 6M (NH4)2S to each centrifuge tube. Record your observation. Centrifuge the mixtures for 3 mins. and decant the supernatant liquid. Add 10 drops of DI water and 10 drops of 6M HNO3. Stir and boil the mixture in a hot water bath for 5 mins. centrifuge the mixture for 3 mins. Decant the supernatant solution from procedure 3. Discard the To each of the supernatant liquid, add 6 drops of 6M H2SO4. Allow themixtures to cool and 5 drops of DI water. To the mixtures in procedure 4, add few drops of concentrated NH3 until the solution becomes basic. Confirm using a litmus paper. Record your observation. Add 1 drop of 5M NaOH and 1 drop of 0.1 M SnCl2 to the centrifuge tube containing Bi3+ ion , centrifuge and decant the supernatant liquid. To…
Please type all of the parts to this question occordingly to the instructions. Here is an example of a formal procedure based off of the experiment presented in Mohrig:Sodium hydroxide (4.6 g) was dissolved in water (25 mL). This solution was added to a 100 mL round bottom flask along with methyl salicylate (2.0 mL) and a stir bar. The mixture was heated at reflux for 15 min and then progressively cooled to 5 °C. The solution was acidified with 3M sulfuric acid (15-20 mL), and the resulting solid was collected by vacuum filtration. The crude salicylic acid was recrystallized from water to yield ???? g of final solid. The melting point and IR were taken to assess purity. Calculate the molarity of the solution of sodium hydroxide that is used.a. M = b. If the original procedure is the base scale (100%), how far are we scaling down the reaction when using 0.75 mL of methyl salicylate? (Example: the original uses 2.0 mL, if we were to use 1.0 mL, we would be scaling the reaction down…
In a GC run, dodecane was used as test solute for a 30 m x 250 ?m i.d. DB-5 column. The dodecane peak eluted at 5.2 min. and the distance between its two inflection points was 4.0 s. This was the number of theoretical plates generated by this column:
1. From 17M glacial acetic acid, how would you perform serial dilution to prepare 1.0 M, 0.50 M, and 0.25 M acetic acid solutions? 2. From 0.50 M NaOH solution, how would you prepare (by dilution) 200 mL of 0.1 M NaOH solution?
3. Assume that in extraction from water into toulene, analyte A has distribution ratio of 10. A 20 mL portion of an aqueous solution of A is extracted with toulene. Which of thw following procedures will result in most efficient removal of A from the aqueous phase into toulene? (Please show the solution of the correct answer) A. 1 extraction with 20 mL of touleneB. 1 extraction with 40 mL of touleneC. 2 extractions with 20 mL of toulene eachD. 4 extractions with 10 mL of toulene each
Objective: To determine the percent NaCl (w/v) of a water sample 5.00 mL sample diluted to 50 mL solution 0.1000 M AgNO3 Volume of AgNO3 trial 1=15.30 mL trial 2=14.90 mL trial 3=15.10 ml
Methodology: Make schematic diagram for the procedure below B. % SO3 determination Dry the soluble sulfate sample at 100° C for 1-2 hours, and cool in desiccator. Weigh out 0.5 – 0.7 g (± 0.3 mg) duplicates sample. Transfer to 400-mL beakers. Dissolve each in 200 mL of dist. H2O + 4 mL of 6 m HCl. Precipitant is prepared by dissolving 1.3 g BaCl2 ∙ H2O in 100 mL water. Filter if solution is not perfectly clear. Heat the BaCl2 solution and sulfate sample solution nearly to boiling, and then add the entire amount to the HOT sulfate sample solution while stirring vigorously. Wash stirring rod with distilled water and include washings in your final mixture. Digest by letting stand 1-2 hours. Overnight standing is acceptable. Filter through an ash less filter paper of fine porosity (Whatman no. 42). Slowly pour the supernatant liquid through the filter paper.
A sample of anhydrous NaHCO3 (FM = 84.007) is suspected to be contaminated with either NaOH (FM = 39.997) or Na2CO3 (FM = 105.989). To verify the suspicion, a 0.7483 g sample was dissolved to prepare a 50.00 mL solution, and a 10.00 mL aliquot was taken to prepare a 100 mL solution, where 25.00 mL was analyzed using double flask method. If the sample requires 0.45 mL of standard 0.0125 N HCl to reach the phenolphthalein endpoint and 35.95 mL to reach the bromcresol green endpoint, calculate the percentage composition (in %w/w) of all the basic components in the sample.
In a similar experiment, the mass of 3 PB tablets was measured to be 3.1823 g. The tablets were crushed, and 2.9801 g of the powder was transferred to a beaker and reacted with HCl. After filtration, the filtrate was transferred to a 50-mL volumetric flask and diluted with water. 10.00 mL of this stock solution was combined with 0.2 M Na3PO4. The resulting precipitate weighed 0.2425 g after drying. What is the mass of BSS per tablet in mg?Round your answer to 1 decimal place.
A sample of anhydrous NaHCO3 (FM = 84.007) is suspected to be contaminated with eitherNaOH (FM = 39.997) or Na2CO3 (FM = 105.989). To verify the suspicion, a 0.7483 g sample was dissolved to prepare a 50.00 mL solution, and a 10.00 mL aliquot was taken to prepare a 100 mL solution, where 25.00 mL was analyzed using double flask method. If the sample requires 0.45 mL of standard 0.0125 N HCl to reach the phenolphthalein endpoint and 35.95 mL to reach the bromcresol green endpoint, calculate the percentage composition (in %w/w) of all the basic components in the sample.