e. Using 'H NMR data of both your product and the starting material (p-toluic acid), describe hovsupports the formation of 4-bromomethylbenzoic acid. Hint: use chemical shift and integrationresponse. AD 2_9 22Temperature 25Spectrometer nmr.bard.edu-vnmrs400Study owner CHEM202Operator CHEM202Sample Name AD 2_9_22Pulse sequernce PROTONDate collected 2022-02-09Solvent dmsoINTEGRAL VALUESIntegralstan(ppm)endvalueANSPOSETI13.098412.1937.5582810.9928.049381.974SS PIPEORGAN37.481557.097881.9942.417162.217653.041PEAK FREUENCIESindexfreg(ppm)intensity7.8051941.02317.7856141.63253.7.2746338.9297.2540734.80633.29542132.32.46825140.6272.46434154.7722.33414129.6671412108.6.42ppm3No BromnePlot dale 2022-02-09Data file /horne/Research/vnmrsys/data CHEM202/CHEM202_AD_2_9_ 22_20220209_01/AD_2_9_22_PROTON_01

Proton NMR spectroscopy is an analytical technique that is used in structural elucidation. It is…

Answered: Using 'H NMR data of both your product…

Using 'H NMR data of both your product and the starting material (p-toluic acid), supports the formation of 4-bromomethylbenzoic acid. Hint: use chemical shift arn

Organic Chemistry: A Guided Inquiry

2nd Edition

ISBN:9780618974122

Author:Andrei Straumanis

Publisher:Andrei Straumanis

ChapterL4: Proton (1h) Nmr Spectroscopy

Section: Chapter Questions

Problem 19CTQ

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Question

e. Using 'H NMR data of both your product and the starting material (p-toluic acid), describe hov
supports the formation of 4-bromomethylbenzoic acid. Hint: use chemical shift and integration
response.

AD 2_9 22
Temperature 25
Spectrometer nmr.bard.edu-vnmrs400
Study owner CHEM202
Operator CHEM202
Sample Name AD 2_9_22
Pulse sequernce PROTON
Date collected 2022-02-09
Solvent dmso
INTEGRAL VALUES
Integral
stan(ppm)
end
value
ANSPOSE
TI
13.0984
12.193
7.55828
1
0.992
8.04938
1.974
SS PIPE
ORGAN
3
7.48155
7.09788
1.994
2.41716
2.21765
3.041
PEAK FREUENCIES
index
freg(ppm)
intensity
7.80519
41.0231
7.78561
41.6325
3.
7.27463
38.929
7.25407
34.8063
3.29542
132.3
2.46825
140.627
2.46434
154.772
2.33414
129.667
14
12
10
8.
6.
4
2
ppm
3
No Bromne
Plot dale 2022-02-09
Data file /horne/Research/vnmrsys/data CHEM202/CHEM202_AD_2_9_ 22_20220209_01/AD_2_9_22_PROTON_01

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