Was your average experimental mass percent of oxygen in potassium chlorate higher or lower than the theoretical value (circle one)? Higher Lower Which of the following sources of error could be used to explain this discrepancy (circle one)? A. The potassium chlorate sample was not heated strongly or long enough. B. Some of the potassium chloride product splattered out of the crucible during the heating process. Explain your choice. Your response should include an analysis of the calculations you performed with your raw data to obtain your experimental % of oxygen.

Organic Chemistry: A Guided Inquiry
2nd Edition
ISBN:9780618974122
Author:Andrei Straumanis
Publisher:Andrei Straumanis
ChapterL3: Carbon (13c) Nmr Spectroscopy
Section: Chapter Questions
Problem 13CTQ
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Experimental Value = 40.767%

Theoretical Value = 39.165%

Was your average experimental mass percent of oxygen in potassium chlorate higher or lower than the
theoretical value (circle one)?
Higher
Lower
Which of the following sources of error could be used to explain this discrepancy (circle one)?
A. The potassium chlorate sample was not heated strongly or long enough.
B. Some of the potassium chloride product splattered out of the crucible during the heating process.
Explain your choice. Your response should include an analysis of the calculations you performed with your
raw data to obtain your experimental % of oxygen.
Transcribed Image Text:Was your average experimental mass percent of oxygen in potassium chlorate higher or lower than the theoretical value (circle one)? Higher Lower Which of the following sources of error could be used to explain this discrepancy (circle one)? A. The potassium chlorate sample was not heated strongly or long enough. B. Some of the potassium chloride product splattered out of the crucible during the heating process. Explain your choice. Your response should include an analysis of the calculations you performed with your raw data to obtain your experimental % of oxygen.
Mass of original KClO3 sample =
Mass of KCl residue =
Mass of Oxygen released =
Mass Percent of Oxygen in KClO3
Average Mass Percent Oxygen =
Sample 1
[Mass of crucible, lid + KCIO3] -
[Mass of crucible + lid] =
33.745 g - 32.721 g = 1.024 g
[Mass of crucible, lid + residue
after 2nd heating] -
[Mass of crucible + lid] =
33.314 g - 32.721 g = 0.593 g
Mass of original KCIO3 sample -
Mass of KCI residue =
1.024 g - 0.593 g = 0.431 g
42.090 +39.444
2
Mass Percent of Oxygen (experim-Mass Percent of Oxygen (experim-
ental) = Mass of Oxygen released /ental) = Mass of Oxygen released
Mass of Potassium chlorate used x Mass of Potassium chlorate used x
100 = 0.431 g / 1.024 g x 100 = 100 = 0.383 g / 0.971 g x 100 =
42.090 %
39.444%
81.534
Sample 2
[Mass of crucible, lid + KCIO3] -
Mass of crucible + lid] =
33.692 g - 32.721 g = 0.971 g
2
[Mass of crucible, lid + residue
after 2nd heating] -
[Mass of crucible + lid] =
33.309 g - 32.721 g = 0.588 g
Mass of original KCIO3 sample -
Mass of KCI residue=
0.971 g - 0.588 g = 0.383 g
= 40.767 %
Transcribed Image Text:Mass of original KClO3 sample = Mass of KCl residue = Mass of Oxygen released = Mass Percent of Oxygen in KClO3 Average Mass Percent Oxygen = Sample 1 [Mass of crucible, lid + KCIO3] - [Mass of crucible + lid] = 33.745 g - 32.721 g = 1.024 g [Mass of crucible, lid + residue after 2nd heating] - [Mass of crucible + lid] = 33.314 g - 32.721 g = 0.593 g Mass of original KCIO3 sample - Mass of KCI residue = 1.024 g - 0.593 g = 0.431 g 42.090 +39.444 2 Mass Percent of Oxygen (experim-Mass Percent of Oxygen (experim- ental) = Mass of Oxygen released /ental) = Mass of Oxygen released Mass of Potassium chlorate used x Mass of Potassium chlorate used x 100 = 0.431 g / 1.024 g x 100 = 100 = 0.383 g / 0.971 g x 100 = 42.090 % 39.444% 81.534 Sample 2 [Mass of crucible, lid + KCIO3] - Mass of crucible + lid] = 33.692 g - 32.721 g = 0.971 g 2 [Mass of crucible, lid + residue after 2nd heating] - [Mass of crucible + lid] = 33.309 g - 32.721 g = 0.588 g Mass of original KCIO3 sample - Mass of KCI residue= 0.971 g - 0.588 g = 0.383 g = 40.767 %
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