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- In the first part of your extraction, you added NaOH until the pH was 8. Why is a pH of 8 desired? Why is this pH 8 desired when isolating or extracting caffeine from a drink?Which analyte gives a positive result for the Molisch Test?1.What is the significance when KD is either a small or large value? 2. Methyl alcohol and ethyl alcohol are poor extraction solvents. Why?3. What is the major disadvantage of using ether as an extracting solvent?
- Why is sodium chloride added before extraction the aqueous layer with DCM? How does magnesium sulfate break emulsions?For a Kjeldahl analysis: you weighed 0.0312 g unknown dried blood sample and digested it with concentrated H2SO4. After the distillation into boric acid solution, Methyl Purple indicator changed its color to green. During titration with 0.0110 M H2SO4 it took 15.35 mL of this H2SO4 solution to bring the color of the mixture to grey-blue. a) What number of moles of H2SO4 reacted? b) What number of moles of boric acid reacted with NH3 during distillation? c) What number of moles of NH3 was produced during distillation? d) What was mass of N in the produced NH3? e) What is %N w/w in the original sample?if 54.9% of ethenol is in the distillate what would be the sloute and the solvent in the mixture? Explain.
- 1. Why are the acidic extracts and the basic extracts cooled before neutralization during Acid/Base extraction experiment? 2. Why was the water used for washing the precipitates on the funnels specified to be cold during Acid/Base extraction experiment.Why does a 70:30 hexane:acetone mixture produce a more effective separation of pigments in spinach compared to a 50:50 hexane:acetone mixture? Explain thoroughly0.2 mL of 1% azide was added to 0.2 mL of 0.5% dye. What is the concentration of the dye now?
- 1. Basically, when is glass stoppered buret used? ______________________________ ____________________________________________________________________ When is rubber stoppered buret used? ____________________________________ ________________________________________________________________________________________________________________________________________ When is a PTFE buret used? _________________________________________________________ _ _________________________________________________________________________________ 2. Describe the recommended method for the manipulation of a buret stopcock during titration. ________________________________________________________________________________________________________________________________________________________________________________________________________________________________________________________________________________ 3. Why is it necessary to completely fill the rubber tubing of the stopcock with the…Which of the following observations is INCORRECT? a. 4-aminophenol: wine red solution in FeCl3 b. Phenol: white precipitate in Br2 in water c. 3,5-dimethyl-1-hexanol: No layer formation in Lucas reagent d. 3,6-dihydroxycycloheptanone: decolorization of solution in KMnO4 testKiko, a Chem 31.1 student, accidentally shuffled two test tubes with different compounds on his way to the laboratory. To confirm the possible identities of the compounds, Kiko added neutral KMnO4 and Lucas reagents to both test tubes labeled A and B. Test tube A gave a brown precipitate in neutral KMnO4 while test tube B produced a purple solution in the same test. Upon subjecting to Lucas Test, both test tubes produced layers. Which of the following are the possible identities of the compounds A and B? a. Sec-butanol and 3-methyl-3-pentanol b. n-propanol and tert-butanol c. isopropyl alcohol and 4-nitrophenol d. hexanol and cyclopentanol