You are performing an aqueous extraction, and you forget which layer is the organic layer and which is the aqueous layer. What is the best way to solve this problem? a. Add a small amount of sodium sulfate - if it dissolves, the layer is water. b. Remove all the solvents via rotary evaporation and start again. c. Pick the top layer, as this is always the organic layer. d. Smell the two layers to see which one is an organic solvent.
You are performing an aqueous extraction, and you forget which layer is the organic layer and which is the aqueous layer. What is the best way to solve this problem? a. Add a small amount of sodium sulfate - if it dissolves, the layer is water. b. Remove all the solvents via rotary evaporation and start again. c. Pick the top layer, as this is always the organic layer. d. Smell the two layers to see which one is an organic solvent.
Chapter81: Extractions, Separations, And Drying Agents
Section: Chapter Questions
Problem 5P
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You are performing an aqueous extraction, and you forget which layer is the organic layer and which is the aqueous layer. What is the best way to solve this problem?
a. Add a small amount of sodium sulfate - if it dissolves, the layer is water.
b. Remove all the solvents via rotary evaporation and start again.
c. Pick the top layer, as this is always the organic layer.
d. Smell the two layers to see which one is an organic solvent.
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