Experiment #10 & #11
The Synthesis of Cobalt Oxalate Hydrate
The Synthesis of a Nitrite Complex February 5, 2012 Chemistry 1211L - 146 - Spring 2012
Procedure
The Synthesis of Cobalt Oxalate Hydrate
Place 100 ml of distilled water in a 250-ml (or 400-ml) beaker. Add 1.26g of oxalic acid dihydrate (H2C2O4.2H2O) and 1 ml of concentrated ammonia. Stir the mixture until the solid has dissolved completely.
Dissolve 2.34 g of cobalt chloride hexahydrate (CoCl2.6H2O) in 100 ml of water in an Erlenmeyer flask. While stirring the oxalic acid solution constantly, add the cobalt chloride solution drop by drop. Let the mixture cool in an ice bath. A precipitate will form slowly.
After the precipitate has had a
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Theoretical yield: 0.900 g
Actual yield: 0.500 g
% yield: 55.6%
For Synthesis of a Nitrite Complex
Equation:
SrCl2.6H2O + NiCl2.6H2O + 6 KNO2 -> K2SrNi(NO2)6 + 4 KCl + 12 H2O
The limiting reagent were SrCl2.6H2O and NiCl2.6H2O.
Theoretical yield: 1.25 g
Actual yield: 0.500 g
% yield:
The protein molecules in many foods provide the amino acid building blocks required by our own cells to produce new proteins. To determine whether a sample contains protein, a reagent called Biuret solution is used. Biuret solution contains copper ions. However, the chemical state of the copper ions in Biuret solution causes them to form a chemical complex with the peptide bonds between amino acids (when present), changing the color of the solution. Biuret solution is normally blue, but changes to pink when short peptides are present and to violet when long polypeptides are present.
Moisten filter paper with a few drops of solvent and turn on water vacuum to fullest extent
Procedure: Using distilled water, premeasured containers and objects determine displacement of fluids and density of objects. Use ice and heat measure temperatures in Celsius, Fahrenheit and Kelvin.
3. Experiment: Use the Gizmo to find the carrying capacity with Ample, Moderate, and Little land. List the carrying capacities below.
What observations can you make regarding the gene pool and gene frequency of the surviving individuals?
a. Change the 24th bead to a different color. What does the sentence say now (re-read the entire sentence)? Does the sentence still make sense?
What do the left and rights sides of the brain do? Which side of the brain does a police sketch artist use when creating a suspect sketch?
1. During gym class, four students decided to see if they could beat the norm of 45 sit‐ups in a minute. The first student did 64 sit‐ups, the second did 69, the third did 65, and the fourth did 67.
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Title: An investigation into the impact of group pressure on an individual’s estimate of the amount of beads in a pot (ginger granules in a jar).
groups. It was conducted to further the research in choice overload and paralysis of the mind.
Students will carefully observe acts of aggression and prosocial behavior on television, report their observations, and analyze their data to draw conclusions.
The luminous yellow flame is smoky because no air is entering the burner and hydrocarbon is converted into carbon dioxide
Wash (swirl and shake) the organic layer with one 10-mL portion of water and again drain the lower aqueous layer. Transfer the organic layer to a small, dry Erlenmeyer flask by pouring it from the top of the separatory funnel. Dry the crude t-pentyl chloride over 1.01 g of anhydrous calcium chloride until it is clear (see Technique 12, Section 12.9). Swirl the alkyl halide with the drying agent to aid the drying.
2) Rinse the solid with about 30 mL of distilled water and decant the liquid from the solid. It is critical that as little solid as possible is lost during this process. Repeat the rinsing two or three times.