Discussion of Results:
In week one we performed a qualitative solubility test of our fats and oils, synthesized our soaps and detergents, and performed a solubility test and lathering test for the soaps and detergents. We wanted to test the solubility of our starting materials of the soap making process to understand the properties of the materials. In our initial solubility test of the starting materials, we found that most of the materials were insoluble. As you can see in Table 2.0, olive oil and vegetable oil were only soluble in toluene and the shortening and lard were only partially soluble in acetone. In order to understand the solubility of the soaps and detergents, after our synthesis and filtration, we performed a qualitative solubility test with each of
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As shown in Table 3.0, it was difficult to stir and combine the shortening and the lard with the sodium hydroxide and glycerol. Though the oil-based soaps were easy to make, they did not yield as much compared to the fat-based soaps. Table 6.0 shows that Soap 3 which was shortening based and Soap 4 which was lard based produced 11.18 g and 11.22 g, respectively. This was a much greater yield than the oil based soaps. Soap 1 which used olive oil yielded 3.154 grams and soap 2 using vegetable oil yielded 1.319 grams. This was something to consider when choosing which starting material to use and depends on whether ease of synthesis or greater yield is more important. The detergent synthesis methods were very similar but method 2 took less steps and was a bit easier than method 1. Table 6.0 shows that detergent 2 had a greater yield, 5.143 grams whereas detergent 1 had a yield of about 4 grams. The lathering test showed that though soaps 3 and 4 produced the most product of the soaps, they did not create many bubbles or a good lather according to Table 7.0. The soaps/detergents that produced the most bubbles were soap 1 which used olive oil followed by detergent 1 and then soap 2
6. The solubility of the solids were tested using a micro tray, by placing them in water and oil to observe their polarity,
Pre-Lab: A) Hydrate- a compound, typically a crystalline one, in which water molecules are chemically bound to another compound or an element. B) Water of hydration (crystallization)- water that is chemically combined with a substance to form a hydrate and can be expelled (as by heating) without essentially altering the composition of the substance. C) Dehydration- the loss or removal of water from something.
The goal of this project was to make, and test four soaps, and two detergents. The purpose of making four different soaps and two detergents was needed in order to decide which one would be best for the environmental group to use in the future that would allow for the safest cleanup of an oil spill while not harming the animals or the environment in the process. It was necessary to test the impact of the four soaps and two detergents by analyzing their different properties based off of their specific characteristics and the wastewater left over from the vacuum filtration procedure. This procedure had to be undertaken in order to confirm which of the soaps and detergents synthesized is most
In this lab we tested how changing the content of the water affects the speed of the alka seltzer dissolving. My hypothesis was that the tap water would dissolve the tablet fastest, the salt water would be second fastest, and the sugar water would be the slowest. I was correct that the tap water would dissolve the fastest, but I was wrong in that the salt water would dissolve faster than the sugar water. I think that our results came out the way they did because of the amount of sugar and salt we put into the water. When we put the sugar and salt into the beakers, we came up with those measurements on the spot. After the salt and sugar had been added, the salt water was very cloudy, but you could barely tell the tap water from the sugar water.
• Bellis, Mary. "The History of Soap and Detergent." About.com Inventors. About.com, 17 June 2015. Web. 14 Jan. 2016.
This could have occurred because of many different errors during the experiment. One of those errors could have been that some of the product might have been left behind in a beaker when it was transferred over into the vacuum filtration considering the fact that the product was a paste and therefore stuck to the beaker. Another error could have occurred during the vacuum filtration. Some of the extremely small particles could have managed to pass through the filter paper therefore causing the overall products final mass to decrease. The percent yield for the soap made from olive oil was extremely large and abnormal.
The proof (twice the % alcohol) starts at its maximum and goes down (as the alcohol evaporates). If we start with a high concentration of alcohol, we will get the azeotrope (95% alcohol, 5% water) for a while, then the concentration will decrease.
Neutrogena uses a slow, more expensive manufacturing process to mold its fragile soap. In choosing this position, Neutrogena said no to the deodorants and skin softeners that many customers desire in their soap. It gave up the large-volume potential of selling through supermarkets and using price promotions. It sacrificed manufacturing efficiencies to achieve the soap’s desired attributes. (trade-offs that protected the company from imitators)
The purpose of this experiment is to identify the periodic trends in the solubility of the alkaline earth metals and compare the results to that of lead
2. (5 pts) List and explain the names and affiliations of the various characters/stakeholders in this story – I’m looking for us to use the story to map out the complexities that are generally associated with solving public health puzzles – the stakeholders you list and explain here should apply to many of the cases we consider going forward.
1. Obtain a sample of the mixture. The mixture you will separate contains three components: NaCl, NH4Cl, and SiO2. Their separation will be accomplished by heating the mixture to sub-lime the NH4Cl, extracting the NaCl with water, and drying the remaining SiO2.
The main objective of the distillation lab was to identify the composition of an unknown binary solution. The only known component is that the boiling point of the two components were at least 40˚C apart in boiling points. Due to the difference in boiling points, fractional distillation would be an easy way to determine the identity of each component of the binary solution. In the experiment, 30mL of the unknown binary solution was ran through the fractional distillation apparatus. As the solution boiled, gas from the unknown solution ran through the column, which had a temperature gradient to allow rapid and repeated distillations, and one of the components were isolated. By recording the temperature and amount of
As mentioned in the discussion, olive oil, vegetable oil, crisco, and lard were soluble in nonpolar solvents and insoluble in polar solvents. This is due to the chemical composition of polar and nonpolar substances which results from the molecular shape as well as properties of dissolving solutes in solution. Polar substances are hydrophilic and contain polar Van Der Waals interactions (intermolecular forces) such as dipole-dipole forces, ion-dipole forces, and hydrogen bonding. Nonpolar substances are hydrophobic and contain non-polar Van Der Waals interactions. ‘Like dissolve like’ is the reason only polar solutes dissolve in polar solvents and why nonpolar solutes dissolve in nonpolar solvents. Molecules with similar polarity have similar intermolecular forces and therefore, can interact with each, or in this case dissolve9. Additionally, the solubility of a compound is determined by the length of the hydrocarbon chain. Long hydrocarbon chains such as the one found in oleic acid makes a compound more insoluble10. Therefore, since the lipids used in this experiment were hydrophobic substances and each lipid has long hydrocarbon chains, the results were consistent with the scientific literature and principles.
Table 2: Consists of color extract taken from a red cabbage for a natural indicator. The pH reading that was measured by using the pH meter and the result of the pH reading to determine whether the solution was acidic or basic.
The purpose of this lab was to create soaps and detergents and test their cleaning ability. We created four different soaps and two detergents using different starting materials composed of oils and fats for the soaps and lauryl alcohol and sulfuric acid for the detergents. Soaps are created by a process called saponification, which is the formation of a salt by combing an acid and a base.1 Soap and detergent are effective cleaning agents because they have hydrophilic and hydrophobic ends.1 The hydrophobic ends interact with the dirt and oil while the hydrophilic ends interact with the water molecules effectively washing the dirt and oil away.2 While soaps and detergents are very similar in their cleaning ability, they have a major difference being that soaps are made from natural products and detergents are made from synthetic materials.3 In order to make the soaps, we used four different starting materials including lard, shortening, olive oil, and vegetable oil.