2. You are given a 50/50 mixture of cyclohexanamine and cyclohexane and asked to purify it by distillation.NH₂CyclohexanamineCyclohexanea) Which component of the mixture has a higher boiling point and why?b) What is the best distillation method to separate this mixture and why?c) Draw a schematic of what you expect a GC spectra of the 3rd fraction of a fractional distillation. Be sureto identify which peak corresponds to which molecule as well as their relative percentages.

Given: 50/50 mixture of cyclohexanamine and cyclohexane

0/50 mixture of cyclohexanamine and cyclohexane and asked NH₂ Cyclohexanamine Cyclohexane onent of the mixture has a higher boiling point and why? est distillation method to separate this mixture and why?

0/50 mixture of cyclohexanamine and cyclohexane and asked NH₂ Cyclohexanamine Cyclohexane onent of the mixture has a higher boiling point and why? est distillation method to separate this mixture and why?

Organic Chemistry: A Guided Inquiry

2nd Edition

ISBN:9780618974122

Author:Andrei Straumanis

Publisher:Andrei Straumanis

ChapterL3: Carbon (13c) Nmr Spectroscopy

Section: Chapter Questions

Problem 16CTQ

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Question

2. You are given a 50/50 mixture of cyclohexanamine and cyclohexane and asked to purify it by distillation.
NH₂
Cyclohexanamine
Cyclohexane
a) Which component of the mixture has a higher boiling point and why?
b) What is the best distillation method to separate this mixture and why?
c) Draw a schematic of what you expect a GC spectra of the 3rd fraction of a fractional distillation. Be sure
to identify which peak corresponds to which molecule as well as their relative percentages.

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