7. In the standardization of ammonium thiocyanate, 15 mL of 0.1 N silver nitrate VS was measured into a glass-stoppered flask, then titrated with ammonium thiocyanate. 8. lodine flask was not used in iodometric titrations. 9. Mohr method was conducted in slightly acidic condition. 10. Acid-base indicator was used in replacement for the adsorption indicator in the titration of Eaians method.

Fundamentals Of Analytical Chemistry
9th Edition
ISBN:9781285640686
Author:Skoog
Publisher:Skoog
Chapter13: Titrations In Analytical Chemistry
Section: Chapter Questions
Problem 13.5QAP
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Answer 7-10 only

Examine the impact of the following circumstance on the PURITY of the sample. Decide whether the
situation will INCREASE, DECREASE, HAVE NO EFFECT, or BE INDETERMINATE. EXPLAIN
THE TREND IN THREE SENTENCES OR LESS IN THE "OTHER" Given Item IN THE OPTIONS
1. The factor used in the computation of %P for calcium carbonate in complexometry is 2.
2. In complexometric titration of calcium in the presence of magnesium, no masking agent was
applied in the solution.
I
3. In the preparation and standardization of disodium edetate, mineral water was used.
4. The standardization of disodium edetate was conducted in acidic media.
5.Alcohol was not added in the standardization of Zinc Sulfate.
6. Titration of halides using argentometry is conducted in the presence of sunlight.
7.In the standardization of ammonium thiocyanate, 15 mL of 0.1 N silver nitrate VS was measured
into a glass-stoppered flask, then titrated with ammonium thiocyanate.
8. lodine flask was not used in iodometric titrations.
9. Mohr method was conducted in slightly acidic condition.
10. Acid-base indicator was used in replacement for the adsorption indicator In the titration of Falans
method.
Compute for the %purity Average%ourity
Blank Determination
Vol of excess titrant
30.00ml.
Transcribed Image Text:Examine the impact of the following circumstance on the PURITY of the sample. Decide whether the situation will INCREASE, DECREASE, HAVE NO EFFECT, or BE INDETERMINATE. EXPLAIN THE TREND IN THREE SENTENCES OR LESS IN THE "OTHER" Given Item IN THE OPTIONS 1. The factor used in the computation of %P for calcium carbonate in complexometry is 2. 2. In complexometric titration of calcium in the presence of magnesium, no masking agent was applied in the solution. I 3. In the preparation and standardization of disodium edetate, mineral water was used. 4. The standardization of disodium edetate was conducted in acidic media. 5.Alcohol was not added in the standardization of Zinc Sulfate. 6. Titration of halides using argentometry is conducted in the presence of sunlight. 7.In the standardization of ammonium thiocyanate, 15 mL of 0.1 N silver nitrate VS was measured into a glass-stoppered flask, then titrated with ammonium thiocyanate. 8. lodine flask was not used in iodometric titrations. 9. Mohr method was conducted in slightly acidic condition. 10. Acid-base indicator was used in replacement for the adsorption indicator In the titration of Falans method. Compute for the %purity Average%ourity Blank Determination Vol of excess titrant 30.00ml.
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