A 1.5 L of organic compound solution contain 8.0 g of benzoic acid. Methyl tert-butyl ether (MTBE) solvent was used to extract the benzoic acid from the organic compounds into a diluted sodium bicarbonate solution via liquid-liquid extraction (LLE) method. The extracted benzoic acid was transformed into sodium benzoate aqueous solution after LLE. Caculate the total amount of the analyte extracted if the LLE process performed with 1:3 ratio for 3 times, with the recovery of 40% for every step.
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- Please help The petition coeficiente between benzene and water for carta iLife is approximately 3.9 .you are given a 0.35 g sample of acetanilide dissolved in 100ml of water Which of the following extraction techniques will give q better recovery of.acetanilide from water A) one extraction with 60ml of benzene or b) two successive extractions with 30ml portions of benzene? Show calculationA mixture is made up of low molecular weight carboxylic acid, alcohol and ester. What one step procedure can you use to extract the ester component from the mixture? Describe the process brieflyWe want to extract terpenoids from an aqueous sample by continuous liquid-liquid extraction. Which of the following solvents is not suitable for this purpose? Why? Propanone (acetone), dichloromethane, heptane.
- Suppose you have an organic sample X that is somewhat soluble in water, even though it issomewhat more soluble in dichloromethane or ether solvents. But if you do a singleextraction, you get only 60% of your material to transfer from the water to the organic layer.How many “washes” would it take to extract over 90% of your organic material extracted fromthe water layer?9.A linear polyester was synthesized from a mixture of diacid and glycol with carboxyl to hydroxyl ratio greater than unity. A sample of the polyester (3.5 g) requires titration with 23 mL of N/50 KOH to reach a phenolphthalein end point. By vapor-pressure osmometry the molecular weight of the polymer was determined to be 12,000. Calculate the average carboxyl functionality of the polymer (that is, average number of carboxyl groups per polymer molecule).6.0 mL of cyclohexanol, 8 mL of 85% phosphoric acid, and 10 drops of sulfuric acid are added to a 50-mL round-bottom flask with boiling chips, and the mixture is distilled into an ice-cooled receiver. The distillate is in the form of a colorless bi-phasic mixture. The cyclohexene upper layer is removed from the water layer, and dried over anhydrous calcium chloride. Isolated is cyclohexene as a clear and colorless foul-smelling liquid. Weighing data is given below. Gross mass: 51.24 g Tare mass: 48.04 g Product mass: 3.2g Question: Calculate the theoretical mass of the cyclohexene product, bearing in mind that the cyclohexanol starting material was measured by volume, not by mass (so you must use the density of cyclohexanol to convert milliliters to grams, before calculating the number of moles). Calculate the percent yield of cyclohexene obtained.
- Twenty grams of tea leaves was extracted with 250.0 mL water. The aqueous extract was then subjected to liquid-liquid extraction using a total volume of 50 mL chloroform organic solvent.Restate the paragraph. The main objective of the laboratory activity was to make aspirin also known as acetylsalicylic acid in its scientific name. It was successfully done as aspirin was synthesized using the combination of salicylic acid and acetic anhydride. In this reaction, salicylic acid's hydroxyl group on the benzene ring interacted with acetic anhydride to generate an ester functional group. This is an esterification reaction that produces acetylsalicylic acid. Sulfuric acid was utilized as a catalyst to start the esterification reaction. Some unreacted acetic anhydride and salicylic acid, as well as sulfuric acid, aspirin, and acetic acid, remained in the solution after the reaction was completed. The process of crystallization was used to obtain pure crystals of a substance from an impure mixture. Upon completion of the lab, analysis, and calculations, , it is evident that the synthesis of aspirin is possible using these methods but that the yield will be relatively lowIf you had performed the extraction with dichloromethane (d 1.33 g/mL) as the organic solvent and just water as the aqueous layer, describe what is the top and bottom layer and which layer would each of the three starting compounds (benzil, benzoic acid, and alizarin) would be found in.
- On a paper, draw a schematic diagram on the Extraction of Saponins from Gugo by Lead Method using the procedures stated below. Procedures (Stas-Otto Method): Extraction of Saponins from the Gugo Bark by Lead Method Extract saponins from gugo by boiling about 10g of small pieces of gugo bark in water. (If necessary, extract first with ether or petroleum ether). Filter and add a neutral lead acetate solution to the aqueous solution; acid saponins, if present, are precipitated as lead salts. To the filtrate (including the washings, concentrated by evaporation), add basic lead acetate to precipitate neutral saponins. Wash the lead precipitate and suspend in water. Decompose by passing H2S Filter PbS and absorbed impurities. Concentrate the filtrate and finally allow to evaporate to dryness or in vacuum over H2SO4. Purify the saponins by CHCl3 and precipitate with ether. Weigh the residue and compute the percentage yield.Write TRUE if the underlined word/phrase makes the statement correct. Otherwise, write the correct WORD/PHRASE that will make the statement true. d. Washing with hot solvent eliminates adhered mother liquor and avoids crystal dissolution. e. To extract a nonpolar organic compound using solvent extraction, the extracting solvent must be nonpolar, and the washing solvent must be also nonpolar. f. Addition of 6.0 M NaCl extracts saponins by converting them to their salt form. g. The stationary phase in the paper chromatography experiment is the filter paper. h. When the spots have low concentration, they will not be observed as visible spots in the chromatogram. i. An isomer in anti-staggered conformation has higher potential energy than the isomer in eclipsed conformation. j. The addition of excess HCl assures that the formation of tert-butyl chloride is favored. k. If the temperature during distillation of crude tert-butyl chloride reached 90°C, the distillate would contain tert-butyl…5.0 mL of 1-butanol was mixed with 10 mL of HCl. The reaction was put on an ice bath and 4 mL of concentrated sulfuric acid was added. This mixture was refluxed for 45 min and then the product was co-distilled with water using a simple distillation apparatus. Water and the product are immiscible. 1-butanol has a molar mass of 74.12 g/mol, a density of 0.810 g/mL, and a boiling point of 118 C. The product has a molar mass of 92.57 g/mol, a density of 0.880 g/mL, and a boiling point of 78 C. What is the nucleophile in this reaction? What is the role of H2SO4 in this reaction? Calculate the theoretical yield for this reaction. Give your answer in grams. Select the following statements that can be said about the reaction shown.