A bottle of NaCl reagent kept in a school lab stockroom was inadvertently contaminated with naphthalene from moth balls used to keep away cockroaches. Since its use is limited to general school purposes the chemical can still be salvaged. Propose a method to remove the naphthalene particles. Justify your answer. Show the laboratory set-up for the purification process using the basic glasswares in general chemistry.
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- Considering the procedure below: “Determination of the concentration of HCl: Pipette 10 mL of hydrochloric acid and transfer to a 100 mL volumetric flask, complete the volume with water and homogenize. Remove a 10 mL aliquot of this solution and transfer it to a second dilution in a 100 mL volumetric flask, complete the volume with water and homogenize. Take a 20 mL aliquot of this last solution and transfer to a 250 mL erlenmeyr and add 20 mL of distilled water and 4 drops of the acid-base indicator. Titrate with a previously standardized 0.100 mol/L sodium hydroxide solution until the indicator turns.” Answer: a) In this titration, the indicator used is phenolphthalein. Discuss the use of this indicator considering its turning range and pH at the stoichiometric point of the titration. Justify. b) Considering that the volume of titrant used was equal to 24.5 mL, calculate the concentration of HCl in the sample in mol/L.2.3 In an experiment the essential oils from herbs, were extracted with water. Explain how you will separate the oils from the water using liquid-liquid extraction. Discuss the procedure, equipment and extraction solvent choice.Direction:A. Create a complete workflow process of producing a Liquid Dosage Form through Extemporaneous Compounding(Laboratory Setting). Use diagrams (boxes and arrows) to signify stepwise and significant procedures. And Provide a one-paragraph description of the workflow by pinpointing the major steps involved in the illustratedextemporaneous compounding. Highlight each step using red. Thank you!!!
- You are employed as a coop student at the Drug and Alcohol Testing Association of Canada (DATAC) developing analytical tests for sports doping agents. You are asked to prepare a procedure for the extraction of methylphenidate, the active compound in Ritalin, from urine samples (consider them as simple aqueous layers, you do not need to consider other components!). The goal of the procedure is to extract the methylphenidate into an organic layer which will then be evaporated, and the residue will be tested for the drug.You find that methylphenidate is highly soluble in 2-methyltetrahydrofuran, a bio-renewable solvent. Draw the structure of 2-methyltetrahydrofuran and give two reasons why it is a good solvent choice for liquid-liquid extraction.You are employed as a coop student at the Drug and Alcohol Testing Association of Canada (DATAC) developing analytical tests for sports doping agents. You are asked to prepare a procedure for the extraction of methylphenidate, the active compound in Ritalin, from urine samples (consider them as simple aqueous layers, you do not need to consider other components!). The goal of the procedure is to extract the methylphenidate into an organic layer which will then be evaporated, and the residue will be tested for the drug.Your colleague is helping you develop the urine test. They suggest that the urine should be adjusted to a pH above 7 before extracting with the organic solvent. Why is this necessary? Support your explanation with a full arrow-pushing mechanism for the reaction that would occur if the pH was below 7. Include all formal charges, intermediates (if applicable) and products.A student rushed through this experiment. Describe the effect that the following procedural changes would have on the percent recovery of acetanilide. Briefly explain the basis of each answer.(a) Rather than adding 0.5-mL portions of boiling solvent to the acetanilide, the student added 5-mL portions of boiling solvent.(b) The student did not pre-heat the gravity filtration apparatus.(c) The student forgot to cool 5 mL of solvent in Part 5 and washed the crystals with room-temperature solvent.
- Your employer hands you a heterogeneous mixture and asks you to isolate all of thehexane that you can from it. After some analysis, you determine that the mixture contains toluene, hexane,benzoic acid, water, sodium chloride, and sand. Explain how you would isolate pure hexane from thismixture. Remember that you can use techniques such as filtration, extractions, and acid/base chemistrythat we learned earlier in this course in addition to distillation. You may need to look up solubilities and/orboiling points online to solve this problem. You only need to isolate the hexane?How much of the suspending agent is needed to prepare a 60-mL preparation of Aluminum hydroxide gel based on this formulation? Ammonium alum 800 g Sodium carbonate 1000g Peppermint Oil 0.01% (0.01 g/100mL) Sodium benzoate 0.1% (0.1 g/100mL) Purified water, qs ad. 2000 mL a. 0.06 g b. 30 g c. 24 g d. 0.006 gWrite TRUE if the underlined word/phrase makes the statement correct. Otherwise, write the correct WORD/PHRASE that will make the statement true. If there are two bold words/phrases in a number, write your answer for EACH of the bold words/phrases 1. 6-hydroxy-1-naphthoic acid is soluble in 5% NaOH and soluble in 5% NaHCO3. 2. The addition of excess charcoal would decrease the % recovery in the purification by recrystallization. 3. If the target compound is contaminated with impurity, the melting point will be higher than the theoretical value and the melting range is large.
- Please help The petition coeficiente between benzene and water for carta iLife is approximately 3.9 .you are given a 0.35 g sample of acetanilide dissolved in 100ml of water Which of the following extraction techniques will give q better recovery of.acetanilide from water A) one extraction with 60ml of benzene or b) two successive extractions with 30ml portions of benzene? Show calculationMAKE A METHODOLOGY : MATERIALS/ REAGENTS WITH SCHEMATIC DIAGRAM . THE PICTURE UPLOADED SERVES AS A GUIDE, DO THE SAME THING BASED FROM THE PIC. Procedure: Place 20 drops of each of 0.2M CuSO4 in a centrifuge tube. Then add 5 drops of freshly prepared 6M (NH4)2S to each centrifuge tube. Record your observation. Centrifuge the mixtures for 3 mins. and decant the supernatant liquid. Add 10 drops of DI water and 10 drops of 6M HNO3. Stir and boil the mixture in a hot water bath for 5 mins. centrifuge the mixture for 3 mins. Decant the supernatant solution from procedure 3. Discard the To each of the supernatant liquid, add 6 drops of 6M H2SO4. Allow themixtures to cool and 5 drops of DI water. To the mixtures in procedure 4, add few drops of concentrated NH3 until the solution becomes basic. Confirm using a litmus paper. Record your observation. Add 1 drop of 5M NaOH and 1 drop of 0.1 M SnCl2 to the centrifuge tube containing Bi3+ ion , centrifuge and decant the supernatant liquid. To…Two group of students wish to analyse caffeine content in tea samples. Group 1 performed the analysis using thin layer chromatography. Group 2 wish to conduct the analysis using analytical instrumentation. Suggest a possible analytical instrument method for Group 2.Briefly explain the procedural steps before instrumentation. List another two applications of this instrument.