e) Determine the Gibbs energy change per mole of reaction. Faraday's constant is 96485 reduction potentials Eco2H2C204= -0.432 V. Indicate whether it is spontaneous or nonspontaneou C/mol and the standard are Emn04-/Mn2+ =1.507 V and
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- A 1.000 g sample containing chlorides, iodides and inert materials was treated with dilute nitric acid followed by AgNO3. A precipitate of AgCl (143.32) and AgI (234.77) was produced and weighs 0.9238 g. On heating in a current of Cl2, the AgI is converted to AgCl, and the resulting product weighs 0.7238 g. Find the percentage of a) NaI (149.89) and b) NaCl (58.44) in the sampleA 0.7352g sample of ore containing Fe3+, Al3+ and Sr2+ was dissolved and made up to 500.00 mL. The analysis of metals was performed by a chemistry using complexation volumetry. Initially, an aliquot of 50.00 mL had its pH adjusted to 1.0 and titrated with a standard solution of EDTA 0.02145 mol/L, requiring 6.95 mL to reach the end point. Subsequently, another 25.00 mL aliquot was buffered at pH=5 and titrated with the same EDTA solution, requiring 6.24 mL to reach the end point. Finally, a third aliquot of 25.00 mL was titrated at pH=11, requiring 11.10 mL of the same EDTA solution to complete the titration. Determine the percentage of each of the metals in the sample Given the molar masses: Fe=55.845 g/mol; Al=26.982 g/mol and Sr=87.620 g/mol.Explain why colour of KMnO4 disappears when oxalic acid is added to its solution in acidic medium.
- Chromel is an alloy composed of nickel, iron and chromium.A 0.6472 g sample was dissolved and diluted to 250 mL. When a50 mL aliquot of 0.05182 M EDTA was mixed with an equal volumeof the diluted sample and all the three ions were chelated, a 5.11 mLback titration with 0.06241 M copper (II) was required.The chromium in a second 50 mL aliquot was masked through theaddition of hexamethylenetetramine, titration of the Fe and Nirequired 36.28 mL of 0.05182 M EDTA.Iron and chromium were masked with pyrophosphate in a third50 mL aliquot and the nickel was titrated with 25.91 mL of theEDTA solution.Calculate the percentage of nickel, chromium and iron in thealloy.An antihistamine sample, brompheniramine maleate, weighing 5.01234 g was dissolved in alcohol and decomposed with metallic sodium. The resulting solution was treated with 12.00mL of 0.3121M AgNO3 to precipitate all of the liberated bromide ions as AgBr. The excess AgNO3 remaining in the solution was titrated with 9.123mL of 0.2181M KSCN to reach the endpoint. What is the %Br in the sample? Br- + Ag+ --> AgBr(s) Ag+ + SCN- --> AgSCN(s) Br = 79.904 g/molDiscuss Quantitative aspects of Electrolysi/
- When I was a boy, I watched Uncle Wilbur measure the iron content of runoff from his banana ranch. He acidified a 25.0-mL sample with HNO3 and treated it with excess KSCN to form a red complex. (KSCN itself is colorless.) He then diluted the solution to 100.0 mL and put it in a variablepathlength cell. For comparison, he treated a 10.0-mL reference sample of 6.80 3 1024 M Fe31 with HNO3 and KSCN and diluted it to 50.0 mL. The reference was placed in a cell with a 1.00-cm pathlength. Runoff had the same absorbance as the reference when the pathlength of the runoff cell was 2.48 cm. What was the concentration of iron in Uncle Wilbur’s runoff ?A 1.509-g samle of a Pb/Cd alloy was dissolved in acid and diluted to exactly 250.0 mL in a volumetric flask. A 50.00-mL aliquot of the diluted solution was brought to a pH of 10.0 with an HCN/NaCN buffer, which also served to mask the Cd2+; 11.56mL of the EDTA solution were needed to titrate the Pb2+. Calculate the percentage of Pb and Cd in the sample.In order to adjust the Potassium Permanganate solution, 0.0544g Na2C2O4 was taken and necessary experimental procedures were performed on it and the titrant consumption was found to be 7.9 mL. Accordingly, what is the concentration of KMnO4?
- The amount of iron in a meteorite was determined by a redox titration using KMnO4 as the titrant. A 0.4185 -g sample was dissolved in acid and the liberated Fe3+ quantitatively reduced to Fe2+, using a reductor column. Titrating with 0.0044 M KMnO4 requires 28.76 mL to reach the end point. Determine the %w/w Fe2O3 in the sample of meteorite. (Fe = 55.845 amu, Fe2O3 = 159.69 g/molSometimes it is not possible to indicate the end point of a titration.a) How can one proceed then and what is the name of the type of titration that can be performed? Briefly describe. An example in which this method can be used is in the determination of mercury, which forms strong complexes with EDTA, but for which there is no suitable indicator that can indicate the end point. b) You are given the task of determining the Hg2 + concentration in a sample solution? After adding an excess of EDTA, the sample solution is titrated with a magnesium solution. 20.00 ml of a 0.0452 M EDTA solution was added to 30.00 ml of sample solutionThe excess EDTA was determined by adding 0.0500 M Mg 2+ solution, consuming 4.37 ml to the end point.Which of the following statements is true regarding permanganimetry? a) Permanganate solution can oxidize water which is catalyzed by the presence of manganese dioxide or manganese ion. b) The light pink endpoint color for permanganimetry tends to fade with time due to the catalytic reaction. c) Standardization of the permanganate titrant is carried out at elevated temperature with sodium oxalate. d) all of these e) none of these