Ir anaylsis of the product and to gove frequinces that i expect to see to predict ir absorption bands for functional groups present within the molecule

Organic Chemistry
8th Edition
ISBN:9781305580350
Author:William H. Brown, Brent L. Iverson, Eric Anslyn, Christopher S. Foote
Publisher:William H. Brown, Brent L. Iverson, Eric Anslyn, Christopher S. Foote
Chapter19: Enolate Anions And Enamines
Section19.9: Crossed Enolate Reactions Using Lda
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I need help predicting the Ir anaylsis of the product and to gove frequinces that i expect to see

to predict ir absorption bands for functional groups present within the molecule 

 

IRil.
IHAMR:Z chem
eral Equation:
Stretch
СНО
+
NaOH (aq)
+ 2 H2Ø
58.05
eral Procedure:
284. 79 g/mo) (A
Transcribed Image Text:IRil. IHAMR:Z chem eral Equation: Stretch СНО + NaOH (aq) + 2 H2Ø 58.05 eral Procedure: 284. 79 g/mo) (A
Synthesis of Dibenzalacetone (1,5-Diphenyl-1A-pentadien-3-one)
By Mixed-Aldol Condensation
General Equation:
СНО
NaOH (aq)
+ 2 H20
+
58.09
184.19 g/mo)
General Procedure:
Into a clean 25 mL round-bottom-flask (RBF) equipped with magnetic stirring bar place 4.0 mL of 10
% sodium hydroxide solution, and add 3.2 mL of 95 % ethanol, 40 mL of benzaldehyde. Finallý add 0.15 mL
of acetone to the reaction mixture. Cap the RBF and mix the reaction mixture continuously for 30 minutes. If
no solid product forms, open the container and scratch inside the RBF, under the liquid with a glass rod. After
30 minutes, remove the liquid from the vial using a Pasteur pipette by squeezing the bulb of the pipette,
pressing the pipette tip flat against the bottom of the vial, and bringing the liquid up while leaving the crystals
Transcribed Image Text:Synthesis of Dibenzalacetone (1,5-Diphenyl-1A-pentadien-3-one) By Mixed-Aldol Condensation General Equation: СНО NaOH (aq) + 2 H20 + 58.09 184.19 g/mo) General Procedure: Into a clean 25 mL round-bottom-flask (RBF) equipped with magnetic stirring bar place 4.0 mL of 10 % sodium hydroxide solution, and add 3.2 mL of 95 % ethanol, 40 mL of benzaldehyde. Finallý add 0.15 mL of acetone to the reaction mixture. Cap the RBF and mix the reaction mixture continuously for 30 minutes. If no solid product forms, open the container and scratch inside the RBF, under the liquid with a glass rod. After 30 minutes, remove the liquid from the vial using a Pasteur pipette by squeezing the bulb of the pipette, pressing the pipette tip flat against the bottom of the vial, and bringing the liquid up while leaving the crystals
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