Please find the Theoretical yield following the oxidation reaction provided below:In a 50 mL round bottom flask dissolve 10 g (10 mmol) of cyclohexanol in 4 mL of ethyl acetate and add a magnetic stirring bar.Add 4g (13 mmol equivalent of KHSO5) to the flask while stirring.Add 0.12 g (2.2 mol) of NaCl followed by 1.5 mL of deionized water.Stir the reaction for 40 minutes at room temperature.Add additional NaCl (0.05 g, 0.7 mmol) and stir for 10 minutes.Add 15 mL of deionized water to dissolve all the salts.Slowly add a spatula tip of solid sodium bisulfite to destroy any excess oxidant.Test the aqueous layer with starch-iodide test paper and add additional sodium bisulfite until this test is negative for oxidant.Extract the product with ethyl acetate (2 X 5 mL), wash with saturated NaCl solution and dry the organic layer over magnesium sulfate.

KHSO5 is potassium peroxymonosulfate. It reacts with NaCl to produce sodium hypochlorite (NaOCl) in…

Answered: Please find the Theoretical yield…

Chemistry

10th Edition

ISBN:9781305957404

Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste

Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste

Chapter1: Chemical Foundations

Section: Chapter Questions

Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...

See similar textbooks

Related questions

Question

100%

Please find the Theoretical yield following the oxidation reaction provided below:

In a 50 mL round bottom flask dissolve 10 g (10 mmol) of cyclohexanol in 4 mL of ethyl acetate and add a magnetic stirring bar.
Add 4g (13 mmol equivalent of KHSO5) to the flask while stirring.
Add 0.12 g (2.2 mol) of NaCl followed by 1.5 mL of deionized water.
Stir the reaction for 40 minutes at room temperature.
Add additional NaCl (0.05 g, 0.7 mmol) and stir for 10 minutes.
Add 15 mL of deionized water to dissolve all the salts.
Slowly add a spatula tip of solid sodium bisulfite to destroy any excess oxidant.
Test the aqueous layer with starch-iodide test paper and add additional sodium bisulfite until this test is negative for oxidant.
Extract the product with ethyl acetate (2 X 5 mL), wash with saturated NaCl solution and dry the organic layer over magnesium sulfate.

Expert Solution

Trending now

This is a popular solution!

Step by step

Solved in 2 steps with 1 images

SEE SOLUTION Check out a sample Q&A here

Knowledge Booster

Learn more about

Need a deep-dive on the concept behind this application? Look no further. Learn more about this topic, chemistry and related others by exploring similar questions and additional content below.

Similar questions