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- Organotin compounds play a significant role in diverse industrial applications. They have been used as plastic stabilizers and as pesticides or fungicides. One method used to prepare simple tetraalkylstannanes is the controlled direct reaction of liquid tin(IV) chloride with highly reactive trialkylaluminum compounds, such as liquid triethylaluminum (Al(CzHs)3). 3SnCl4 + 4Al(C2H5)3 → 3Sn(C2H5)4 + 4AlCl3 In one experiment, 0.160 L of SnCl4 (d= 2.226 g/mL) was treated with 0.346 L of triethylaluminum (Al(C2H5)3); d = 0.835 g/mL). What is the theoretical yield in this experiment (mass of tetraethylstannane, Sn(C2H5)4)? If 0.257L of tetraethylstannane (d= 1.187 g/mL) were actually isolated in this experiment, what was the percent yield?For butenafine, develop a synthesis that starts with napthalene and benzene. (aromatic methyl groups can be converted to alkyl bromides using Br2/light, and aldehydes by heating the alkyl bromide in DMSO, eg. ArCH3 to ArCH2Br then to ArCHO).Explain wurtz reaction with suitable reaction.
- Organotin compounds play a significant role in diverse industrial applications. They have been used as plastic stabilizers and as pesticides or fungicides.One method used to prepare simple tetraalkylstannanes is the controlled direct reaction of liquid tin(IV) chloride with highly reactive trialkylaluminum compounds, such as liquid triethylaluminum (Al(C2H5)3). 3SnCl4 + 4Al(C2H5)3 3Sn(C2H5)4 + 4AlCl3 In one experiment, 0.230 L of SnCl4 (d = 2.226 g/mL) was treated with 0.396 L of triethylaluminum (Al(C2H5)3); d = 0.835 g/mL). If 0.335 L of tetraethylstannane (d = 1.187 g/mL) were actually isolated in this experiment, what was the percent yield?Write out the reaction of Bromination of E-stilbene using chemdraw (ACS 1996 format). Include all reagents, products, solvents, reaction temperature and yield. Reagents used include glacial acetic acid, E-stilbene, and pyridinium perbromide, otherwise known as PHPB. Glacial acetic acid: 10mL Stilbene: 0.5g Perbromide: 1.0g Product yield (Precipitate) weight: 0.63gDescribe how the product is purified. 4,4'-DIBROMOBIPHENYL [Biphenyl, 4,4'-dibromo-] Submitted by Robert E. Buckles and Norris G. Wheeler1. Checked by R. S. Schreiber, Wm. Bradley Reid, Jr., and Robert W. Jackson. 1. Procedure In a 15-cm. evaporating dish is placed 15.4 g. (0.10 mole) of finely powdered biphenyl (Note 1). The dish is set on a porcelain rack in a 30-cm. desiccator with a 10-cm. evaporating dish under the rack containing 39 g. (12 ml., 0.24 mole) of bromine. The desiccator is closed, but a very small opening is provided for the escape of hydrogen bromide (Note 2). The biphenyl is left in contact with the bromine vapor for 8 hours (or overnight). The orange solid is then removed from the desiccator and allowed to stand in the air under a hood for at least 4 hours (Note 3). At this point, the product weighs about 30 g. and has a melting point in the neighborhood of 152°. The crude 4,4'-dibromobiphenyl is dissolved in 75 ml. of benzene, filtered, and cooled to 15°. The…
- Why do we need to allow the solution of KF reagent to stand overnight before standardizing? if copied from google please paraphraseII. Alcohols in Synthesis B.) How are alcohols used to make ethers in the Williamson ether synthesis? How do you design the synthesis of ethers using both acidic and basic Williamson ether synthesis strategies?The product of reaction between acetone and bromine (excess) with KOH excess is A. Ch2BrCOCh3 B. ChBr3 C.ChBr2COCH3 D.CBr3COCH3 E.Ch2BrCOCHBr2
- Please complete reactions in clear handwritten of all subpartsChemistry please provide the flow of electrons aswell!! thank you! using the starting material (on the left) to determine the sythetic route which will be the most reaosnable and effective to theres none, you have to start witth the begin products to get to finish needed by using the minmium reagents and reactions needed to get to the final productplease quickly thanks ! 3.Please write out the major reaction and side-reaction in the preparation of ter-butyl.chloride, and write out the key points to use separation funnel in this process.