Sources of Error Determine the relationship between the observed/apparent value (EX) VERSUS that of the true value (ET) for the quantity being sought by writing either <, >, or = on the space provided TOPIC: Measured mass of the crucible After heating, the crucible was weighed without cooling. EX _____ ET TOPIC: Measured mass of the precipitate Filter paper was dried prior to filtration. EX _____ ET

Sources of Error Determine the relationship between the observed/apparent value (EX) VERSUS that of the true value (ET) for the quantity being sought by writing either <, >, or = on the space provided TOPIC: Measured mass of the crucible After heating, the crucible was weighed without cooling. EX _ ET TOPIC: Measured mass of the precipitate Filter paper was dried prior to filtration. EX _ ET

Fundamentals Of Analytical Chemistry

9th Edition

ISBN:9781285640686

Author:Skoog

Publisher:Skoog

Chapter8: Sampling, Standardization, And Calibration

Section: Chapter Questions

Problem 8.6QAP

See similar textbooks

Sources of Error

Determine the relationship between the observed/apparent value (E_X) VERSUS that of the true value (E_T) for the quantity being sought by writing either <, >, or = on the space provided

TOPIC: Measured mass of the crucible

After heating, the crucible was weighed without cooling. E_X _____ E_T

TOPIC: Measured mass of the precipitate

Filter paper was dried prior to filtration. E_X _____ E_T

Expert Solution

This question has been solved!

Explore an expertly crafted, step-by-step solution for a thorough understanding of key concepts.

SEE SOLUTION Check out a sample Q&A here

Step 1

VIEW

Step 2

VIEW

Step 3

VIEW

Step by step

Solved in 3 steps

SEE SOLUTION Check out a sample Q&A here

Knowledge Booster

Learn more about

Need a deep-dive on the concept behind this application? Look no further. Learn more about this topic, chemistry and related others by exploring similar questions and additional content below.

Similar questions

An analyst determines the Cl^- content of rain water with ion chromatography. The data for the calibration line in the range 5 to 50 milli equivalents per liter (mEq/L) is shown in the table below. Additionally, a blank sample was analysed 5 times and the following results obtained: 1.1, 0.5, 0.1, 0.9 and 1.2 ppm Ct Calculate the detection limit (DL) for the method with a 98.3% confidence level. Use ALL data and show equations
The concentration of purified OXA-M290 is tested with a BCA assay. Serial dilutions of a bovine serum albumin (BSA) stock solution are prepared, then pipetted into a 96-well plate; each dilution of the BSA standard is tested in triplicate. Then, bicinchoninic acid and Cu2+ ions are added to all of the wells of the plate. After incubating the plate for 1 hour, a microplate reader is used to measure the absorbance of all of the wells in the plate at 560 nm. This generates the following data: BSA conc. (μg/mL), Replicate 1 Absorbance, Replicate 2 Absorbance, Replicate 3 Absorbance 40, 1.360, 1.403, 1.481 20, 0.750, 0.745, 0.810 10, 0.380, 0.344, 0.398 5, 0.198, 0.160, 0.183 2.5, 0.090, 0.100, 0.085 1.25, 0.038, 0.043, 0.051 0.625, 0.024, 0.028, 0.019 Prepare a calibration curve using these data. You can use Excel, R, SPSS or an equivalent graphing software. In this graph, plot absorbance (y-axis) against the concentration of the protein standard (x-axis). Calculate and plot…
A 5.00 (±0.01) mL5.00 (±0.01) mL Class A transfer pipet is used to transfer 5.00 mL5.00 mL of a 0.253 (±0.003) M0.253 (±0.003) M Cu2+Cu2+ stock solution to a 100.00 (±0.08)100.00 (±0.08) Class A volumetric flask. Deionized water is used to bring the flask to volume. Calculate the concentration of the diluted soluion in the volumetric flask and report its absolute uncertainty.
A new method is proposed to simultaneously detectand separatefour foodadditives by reversed-phase liquid chromatography. The data were obtained using theliquid chromatographic column with a flow rate of 0.5 mL per min and with the followingparameters: Pore size 100 A Particle Size 3.5 Internal diameter 4.6 mm Length 150 mm The food additives found in the sample resulted in the following data: ( see image for table) a.Calculate the number of plates from each peak. b.Calculate the plate height for the column. c.Retention factor for each peak.
A 0.500g sample is analyzed spectrophotometrically for manganese by dissolving it in acid and transferring to a 250 mL flask and diluting to volume. Three aliquots ae analyzed by transferring 50 mL portions with a pipet to 500 mL Erlenmeyer flask and reacting with an oxidizing agent, potassium peroxydisulfate, to convert the manganese to permanganate. After reaction, these are quantitatively transferred to 250 mL volumetric flasks, diluted to volume and measured spectrophotometrically. By comparison with standards, the average concentration of the final solution is determined to be 1.25 x 10^-5M. What is the percent manganese in the sample?
The answer with a BCA table for both parts would be great, thank in advance for the help. btw, this is a pre test that isn’t graded
In a chromatography experiment, a solution containing 0.083 7 M X and 0.066 6 M S gave peak areas of AX = 423 and AS 5 347. (Areas are measured in arbitrary units by the instrument.) To analyze the unknown, 10.0 mL of 0.146 M S were added to 10.0 mL of unknown, and the mixture was diluted to 25.0 mL in a volumetric flask. This mixture gave the chromatogram in Figure 5-8, with peak areas AX = 553 and AS = 582. Find the concentration of X in the unknown.
I got a task in analytical chemistry to calibrate, standardize, verify and validate an analytical balances
4.Consider the peaks for pentafluorobenzene and benzene in the gas chromatogram shown here. The elution time for unretained solute is 1.06 min. The open tubular column is 30.0 m in length and 0.530 mm in diameter, with a layer of stationary phase 3.0 μm thick on the inner wall. a) Measruing the width, w, at the baseline on the chromatogram, find the number of plates for these two compounds b) Use your answer to (a) to find the resolution between the two peaks c) Using the number of plates N=sqrtN1*N2 with the values from (a) calcuate what the resolution should be and compare your answer with the measured resolution in b
A variation of the indicator-dilution method (see preceding problem) is used to measure total blood volume. A known amount of a tracer is injected into the bloodstream and disperses uniformly throughout the circulatory system. A blood sample is then withdrawn, the tracer concentration in the sample is measured, and the measured concentration [which equals (tracer injected)/(total blood volume) if no tracer is lost through blood vessel walls] is used to determine the total blood volume.In one such experiment, 0.60 cm3 of a solution containing 5.00 mg/L of a dye is injected into an artery of a grown man. About 10 minutes later, after the tracer has had time to distribute itself uniformly throughout the bloodstream, a blood sample is withdrawn and placed in the sample chamber of a spectrophotometer. A beam of light passes through the chamber, and the spectrophotometer measures the intensity of the transmitted beam and displays the value of the solution absorbance (a quantity that…
A fly ash aerosol of monodisperse particles with a density of 2.0 g/mL and particle diameter of 10.0 mm has a concentration of 1000.0 mg/m3. Calculate the settling velocity in cm/s and the settling rate in g/m2-s. Please answer very soon will give rating surely
Sources of Error Determine the relationship between the observed/apparent value (EX) VERSUS that of the true value (ET) for the quantity being sought by writing either <, >, or = on the space provided TOPIC: Determination of % SO32- Question 1 Not all solid was transferred during the filtration of the precipitate. EX ___ ET TOPIC: Measured mass of the crucible Question 2 After heating, the crucible was weighed without cooling. EX ___ ET TOPIC: Measured mass of the precipitate Question 3 Filter paper was dried prior to filtration. EX ___ ET