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- 6. The quantitative determination of pyridoxine hydrochloride can be carried out by methods: A. Complexometry B. Argentometry C. Alkalimetry D. Acid-base titration in a protogenic solvent medium E. Acid-base titration in a profile solvent mediumThe Kjedahl procedure was used to analyze 256 µL of a solution containing 37.9 mg protein/mL. The liberated NH3 was collected in 5.00 mL of 0.033 6 M HCl, and the remaining acid required 6.34 mL of 0.010 M NaOH for complete titration. What is the weight percent of nitrogen in the protein? wt%(b) The distribution ratio for X between n-hexane and water is 8.9. Calculate the concentration of X remaining in the aqueous phase after 50.0 mL of 0.200 M X is treated by extraction with the following quantities of n-hexane?
- Calculate the diesel index of the sample that its aniline point is 104°F and thedensity is 0.86 g/ml.1. A 1.2-gram sample of lanolin was treated with Wij’s solution and excess potassium iodide solution. The liberated iodine reacted with 30 ml of 0.1 N sodium thiosulfate solution. If the iodine value was determined as 12.69, what is the volume used in blank titration? 2. A fat sample with combination of acids contain standard hydrochloric acid for blank and sample with 8mL and 5mL respectively. The normality of the standard hydrochloric acid is 0.93N and the weight of the sample is 3 grams. Calculate the saponification value. 3. A 3.50-gram sample of Streptomycin powder was tested for its water content. If the water equivalence factor of the KF reagent was 4.6, what is the percentage water content of the sample if 9.2 ml of the KF reagent was used? 4. A 500mg oil sample is taken from a conical flask and is dissolved in 50mL distilled alcohol. An indicator is added and is then titrated against 0.112N KOH until a slight pink color appears. It took 17.6mL of the titrant to reach the…You are given the suggestion that a 0.15 ppm quinine aqueous solution is a good concentration to shoot for in the experiments, but quinine fluoresces best when it is acidified to 0.10 M H2SO4. Describe how to make 100 mL of the recommended solution starting with quinine sulfate (actually, quinine hemisulfate salt monohydrate). Assume you also have 1.0 M sulfuric acid and de-ionized water.
- What volume of CHCl3 is needed to decrease the concentration of compound X to 1.00 x10-4 M if it is performed the extraction of 25.0 mL from a 0.0500 M solution with (a) 25.0 mL portions of CHCl3, (b) 10.0 portions mL and (c) 2.0 mL portions of CHCl3 ?. (KD 9.6)A fish sample was analyzed for crude protein content using the Kjeldahl method. Thefollowing data were recorded: Moisture content 10.0%Weight of sample 2.15 gNormality of HCl used for titration 0.121 NHCl used for sample 28.5 mLHCl used for reagent blank 0.2 mL Calculate crude protein content on wet weight basis of the fish sample, assuming fishprotein contains 20% nitrogen.The distribution coefficient for X between chloroform and water is 9.6. What volume of CHCl3 is required to decrease the concentration of X to 1.0 × 10-4 if 25.0 ml of 0.0500 M X is extracted witha) 25.0 ml portions of CHCl3b) 10.0 ml portions of CHCl3c) 2.0 ml portions of CHCl3
- Accurately weigh out about 6g copper(ii) sulfate crystals into a weighing boat. Use the copper(ii) sulfate crystals to make up 250cm3 of standardized copper (ii) sulfate solution Pipette 25cm3 of this solution into a conical flask Add 1.5g potassium iodide and swirl thoroughly Titrate this solution with standard 0.1 moldm-3 Na2S2O3 in a burette. When the iodine color fades, add 1 cm3 starch indicator. Use your titration data below to calculate the percentage by mass of copper in the copper(ii) sulfate crystals.Betnovate-RD® contains 0.025% w/w betamethasone valerate in a water-miscible basis. How much betamethasone valerate is contained in a 100g tube?1. Why is there a need to correct conductivity of the sample solution?2. Cite three possible sources of error in the experiment and discuss their effects on the computed ionization constant of the acetic acid. (See details below----- literature value- Ki, acetic acid= 1.75 x 10^-5). 3. What is the effect of dilution on the fraction of the acetic acid ionized?