The following experimental process steps have been made to determine the hardness of water. Accordingly, 100 mL sample was acidified with a few drops of 6 M HCl and boiled for a while to remove the CO2 in it. Then add a few drops of methyl red 6pH: 4.2-6.3) to the cooled sample and neutralize the solution with 0.1M NaOH, then add 2 ml of 0.01M pH10 buffer and 4-5 drops on it. EBT indicator was added and the solution was titrated with 0.0086M EDTA until the color turned blue. Since the consumption of titrant is 11.44mL, calculate the amount of Ca in the water in terms of mg CaCO3. (Ca: 40, C: 12, 0:16) A. 8,75 O B. 9,83 C. 10,44 D. 10,35 Reset Selection

The following experimental process steps have been made to determine the hardness of water. Accordingly, 100 mL sample was acidified with a few drops of 6 M HCl and boiled for a while to remove the CO2 in it. Then add a few drops of methyl red 6pH: 4.2-6.3) to the cooled sample and neutralize the solution with 0.1M NaOH, then add 2 ml of 0.01M pH10 buffer and 4-5 drops on it. EBT indicator was added and the solution was titrated with 0.0086M EDTA until the color turned blue. Since the consumption of titrant is 11.44mL, calculate the amount of Ca in the water in terms of mg CaCO3. (Ca: 40, C: 12, 0:16) A. 8,75 O B. 9,83 C. 10,44 D. 10,35 Reset Selection

Fundamentals Of Analytical Chemistry

9th Edition

ISBN:9781285640686

Author:Skoog

Publisher:Skoog

Chapter7: Statistical Data Treatment And Evaluation

Section: Chapter Questions

Problem 7.26QAP

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The following evidence was obtained from an experiment to determine the solubility of calcium chloride at room temperature. A sample of saturated calcium chloride solution was evaporated to dryness, and the mass of solid residue was measured.EvidenceVolume of solution (mL) = 15.0Mass of empty beaker (g) = 90.54Mass of beaker and residue (g) = 101.36The solubility of calcium chloride is g/100 mL
Although other solvents are available, dichloromethane(CH₂Cl₂) is still often used to “decaffeinate” drinks because thesolubility of caffeine in CH₂Cl₂ is 8.35 times that in water.(a) A 100.0-mL sample of cola containing 10.0 mg of caffeine is extracted with 60.0 mL of CH₂Cl₂. What mass of caffeine re-mains in the aqueous phase? (b) A second identical cola sampleis extracted with two successive 30.0-mL portions of CH₂Cl₂.What mass of caffeine remains in the aqueous phase after each extraction? (c) Which approach extracts more caffeine?
Hexanoic acid was added to an immiscible biphasic solvent system, water and CCl4 at 20.0OC and the equilibrium concentrations of hexanoic acid were determined to be 3.66 g/L in H2O and 67.0 g/L in CCl4. Caluclate the distrubution coeffiecent (D2) of hexanoic acid in water with respect to CCl4.
One litre of a saturated aqueous solution of Ag2SO4 (MW = 311.79 g mol- 1) at 25 °C is evaporated to dryness. 4.844 g of Ag2SO4 residue was produced. What is the solubility product (Ksp)?
To determine the fluoride content in an aqueous and chloride-containing preparation of ammonium fluoride, the following analysis was performed. 105.2 mg of the preparation was dissolved in 100.0 mL of water. Then a 300 mL 40 mM lead chloride solution was added, whereby all fluoride ions were precipitated out of the solution in the form of the sparingly soluble salt PbClF (s). The precipitate was separated and washed at 15 degrees with a lead fluoride chloride saturated solution and dried at 130 degrees. The precipitate weighed 651.3 mg. a) Calculate the fluoride content (as % by weight F) in the preparation.b) Determine the purity of the ammonium fluoride preparation
A polymer of large molar mass is dissolved in the organic solvent m-cresol (C7H8O) at 25 °C, and the resulting solution rises to a final height of 13.4 cm above the level of the pure solvent, as solvent molecules pass through a semipermeable membrane into the solution. If the solution contains 5.24 g polymer per liter, calculate the molar mass of the polymer. Take the density of the solution to be 1.03 g cm-3.
What wt of magnetite should be taken for analysis in order that after converting to a precipitate of Fe2O3.xH2O, the percentage of Fe3O4 in the sample can be found by multiplying the wt in grams of the ignited precipitate (Fe2O3) by 100.
A solution is prepared by dissolving 40.00 g of NaCl (f.w. = 58.44 g mol–1), a non-volatile solute, in enough water (m.w. = 18.02 g mol–1) to result in exactly 1 L of solution at 25 °C. Assume the density of the solution is that of pure water (dsolution = 1.000 g mL–1). The ebullioscopic constant (Kb) for water is 0.513 °C m–1. The cryoscopic constant (Kf) for water is 1.86 °C m–1. The vapor pressure of pure water is 0.0313 atm. Find the freezing point of the solution(in C to 2 decimal places)
A solution is prepared by dissolving 40.00 g of NaCl (f.w. = 58.44 g mol–1), a non-volatile solute, in enough water (m.w. = 18.02 g mol–1) to result in exactly 1 L of solution at 25 °C. Assume the density of the solution is that of pure water (dsolution = 1.000 g mL–1). The ebullioscopic constant (Kb) for water is 0.513 °C m–1. The cryoscopic constant (Kf) for water is 1.86 °C m–1. The vapor pressure of pure water is 0.0313 atm. Find the vapor pressure of the solution to 3 decimal places in atm.
A solution is prepared by dissolving 40.00 g of NaCl (f.w. = 58.44 g mol–1), a non-volatile solute, in enough water (m.w. = 18.02 g mol–1) to result in exactly 1 L of solution at 25 °C. Assume the density of the solution is that of pure water (dsolution = 1.000 g mL–1). The ebullioscopic constant (Kb) for water is 0.513 °C m–1. The cryoscopic constant (Kf) for water is 1.86 °C m–1. The vapor pressure of pure water is 0.0313 atm. Determine the following: Boiling point of solution (in °C to two decimal places) Freezing point of solution (in °C to two decimal places) Vapor pressure of the solution (in atm to three decimal places) Osmotic pressure (in atm to three decimal places)
An excess amount of Ba(NO3)2 was added to 2 liters of water at 25 oC until the solution is saturated. Because Ba(NO3)2 is only slightly soluble in water, the excess Ba(NO3)2 was filtered out to get a solid-free mixture. The proponents of the experiment thought about using the concept of colligative properties, specifically boiling point elevation, to determine Ksp. It was observed in their experiments that the solution boils at 100.15 deg C. Kb of water = 0.51 K-kg/mol. Barium nitrate dissociates using: Solve the ff: a) Amount of Ba(NO3)2 dissolved in grams. MW of Ba(NO3)2 = 261.3 g/molb) Solubility product, Kspc) Vapor pressure of the solution in kPa
1.1The Ksp of Ca3 (PO4 ) 2 is 1.3 × 10−26 . Estimate the solubility of this salt in units of g. L −1 . You must show any reaction equation(s) that you may think are necessary. 1.2 If a sample of solid Ca3(PO4)2 is stirred into exactly one litre of a 0.550M solution of Na3PO4, how will the solubility of the salt compare with the answer that you have obtained in question 1.1? Explain you answer in a short sentence.