The substance to be analyzed – is white, highly soluble in water salt. Interaction with water solution of sodium hydroxide leads to formation of white precipitate, soluble in reagent surplus. Addition to the substance solution of barium chloride leads to appearance of white precipitate (insoluble in hydrochloric acid). Spot assay (drop reaction, filter paper test) with alizarin gives red spot. What kind of salt is this? Al2(SO4)3 - MnCl, ZnSO4 Mn(NO3)2
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- Which of the following steps would affect both yield and purity during the extraction of ovalbumin?a. Washing the precipitate with ethanol before storageb. Using KCl instead of NaCl for the storage solution c. Adding (NH4)2SO4 in bulk instead of in incrementsd. Making use of a centrifuge with a larger diameter1. In using the centrifuge machine, how will this be remedied if there are only 3 separate liquid mixtures, in order to separate their respective precipitates 2. what is the extracting solvent for iodide and bromide ions? 3.What is the oxidation number of molybdenum in (NH4)3PO4.12MoO3 ? 4. Give the change in oxidation number for the element in the anion in group V which shows extensive change in color because it has undergone oxidation? 5. Determine the oxidation number of the Arsenic in Magnesium Ammonium Arsenate?A 500.0mg of butter was warmed and shaken vigorously with water. The undissolved material was removed by filtering and the aqueous portion was made 1.0M in HNO3 and 0.025M in Fe(NO3)3. This acidified solution was treated with 10.00ml of 0.1755M AgNO3 to precipitate the chloride ion and, after the addition of a small amount of nitrobenzene, 14.22ml of 0.1006M KSCN was required to back titrated the excess Ag+. Calculate the % NaCl in the butter.
- Prepare a written copy of the complete separation scheme for a solution that contains Ag+, Fe3+, Cr3+, Ni2+, Zn2+, and Ba2+. Make sure that your separation scheme includes: separation of each ion into its own individual sample AND precipitation BEFORE a confirmation test is done all phases and visible colors, if applicable reagents and conditions necessary to carry out each step balanced equations, including phases, for each stepInclude relevant qualitative test(s) in your explanation in the separation of benzoic acid from NaCl in aqueous solutionIn a separate experiment, the lab partners I. Goofed and T. Klutz treat their unknown with HCl and obtain a precipitate. They treat their precipitate with hot water and decant the supernatant. On treatment of this solid with ammonia, it dissolves. On careful acidification with HNO3 a white precipitate forms. They report that their unknown contains silver. They receive only partial credit. Why?
- Volumetric Analysis The mass of KHC8H4O4 is measured to the nearest milligram; however, the volume of water in which it is dissolved is never of concern—water is even added to the wall of the Erlenmeyer flask during the titration. Explain why water added to the KHC8H4O4 has no effect on the data, whereas water added to the NaOH solution, may drastically affect the data.The standardization of same titrant during the determination of BOD5 of water sample was done separately for Day 1 and Day 5. Upon standardization, it turned out that the concentration of the titrant in Day 1 is higher than the concentration of the same batch of titrant in Day 5. How would you explain this discrepancy? The water used to prepare the Na2S2O3 solution was not boiled resulting to proliferation of bacteria. Too much starch indicator was added in the conical flask. Sulfuric acid was added first before potassium iodide. There were bubbles at the tip of the burette during titration.FeCl3 and MgCl2 solution was prepared by dissolving FeCl3 (AR) and MgCl2 (AR) in distilled water. Secondly, under rapid stirring, NaHCO3 powder was slowly added to the above solution to the desired basicity (B = 1) which had been proved to be the optimal B for turbidity removal. Thirdly, Na2HPO4 (AR) was added to the PFMC solution as a stabilizer ([Na2HPO4]/([Fe] + [Mg]) = 0.08). i. The the chemical equation of the Synthesis. ii How much weight need to put NaHCO3 above solution the desired basicity (B=1) iii. How much weight need to put Na2HPO4 on PFMC solution refering ([Na2HPO4]/([Fe] + [Mg]) = 0.08).
- Write a flow diagram Prepare a written copy of the complete separation scheme for a solution that contains Ag+, Fe3+, Cr3+, Ni2+, Zn2+, and Ba2+. Make sure that your separation scheme includes: separation of each ion into its own individual sample AND precipitation BEFORE a confirmation test is done all phases and visible colors, if applicable reagents and conditions necessary to carry out each step balanced equations, including phases, for each stepwhy is it necessary to test the ph? PROCEDURE To a six inch test tube was added thiamine hydrochloride (0.65 g), followed by water (2mL). The mixture was gently shaken until homogeneous, and then ethanol (7.5 mL)was added. Finally, sodium hydroxide (10%, 1.5 mL) was added and the mixture wasgently stirred to ensure complete mixing.Benzaldehyde (3.8 mL) was then added at room temperature in one portion with gentlestirring. The pH of the resulting reaction mixture was determined and adjusted to >10by dropwise addition of 10% sodium hydroxide.On shaking a binary mixture in a separatory funnel, an emulsion is formed; briefly describe three methods by which you can break the emulsion.