Which characteristic of a precipitate doesn’t do well for gravimetric analysis. a Readily filtered and washed free of contaminants b Of sufficiently high solubility (Ksp) c Unreactive with constituents of the atmosphere and high purity d Of known composition after it is dried or, if necessary, ignited. e None of the above
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Which characteristic of a precipitate doesn’t do well for gravimetric analysis.
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- Which among these is/are properties for the type of precipitate required in gravimetric analysis? Hygroscopic Known composition Reactive with atmospheric constituents Large particlesWhich of the following is not one of the properties of the precipitate in the gravimetric analysis method?A.Should be easily drainedB. resolution should be lowC. must be volatileD. should not react with atmospheric componentsSources of Error Determine the relationship between the observed/apparent value (EX) VERSUS that of the true value (ET) for the quantity being sought by writing either <, >, or = on the space provided. TOPIC: Measured mass of the precipitate 1. Overignition which causes the conversion of BaSO4 precipitate to BaO. EX _____ ET2. Precipitate was not washed thoroughly. Ex _____ ET TOPIC: Standardization of Titrant 3.Distilled water was not equilibrated to room temperature before the preparation of NaOH titrant. EX _______ ET
- The chloride in the sample is to be determined gravimetrically by precipitating and weighing AgCl. What weight in grams of sample should be taken so that the percentage of Cl is obtained by simply multiplying the weight of the AgCl precipitate by 10?Make an schematic diagram for procedure below: B. %SO3 determination Transfer all precipitate to the filter paper avoiding any loses during the filtration procedure. One may use a rubber policeman to scrape remaining precipitate in the beaker. Wash the precipitate in the beaker 3x with hot water before transferring to the filter paper. Test the washings with 0.1 M AgNO3 Cloudiness indicates presence of chloride ions; therefore there is a need to wash more the precipitate. Carefully lift the paper out of the funnel, fold it as demonstrated by your instructor and transfer it onto the constant weighed crucible. Dry the crucible cautiously with a small flam, as instructed by your instructor. The flame should be directed at the top of the container, and the lid should be off. Avoid spattering. After drying, char the filter paper by increasing the flame temperature. The crucible should have free access to air. The lid should be kept handy to smother the filter paper in case it catches fire.…Which of the following co-precipitates is minimized by washing? a. Mixed-crystals b. Adsorbed impurities c. Mechanically entrapped particles d. Occluded particles
- Contamination of precipitate by co-precipitation can be minimized by (tick all that may apply) A. Digestion B. Peptization C. Washing D. Re-precipitationIt is required to know the concentration of an aqueous solution of H2SO4 that appeared in the laboratoryChemistry III and it's unlabeled. To this end, a student of analytical chemistry carried out the followingProcedure: He took 5.00 mL of a fresh and standardized solution of 0.525M NaOH and brought them to a250.0 mL balloon to be completed with distilled water. Subsequently, he poured 15.00 mL of the solutionH2SO4 of unknown concentration in an Erlenmeyer flask and added 2 drops of phenolphthalein.Using a burette filled with the last NaOH solution, he noticed that when adding 39.40 mL of the hydroxidethe Erlenmeyer solution reached a faint but permanent pink. With the above dataDetermine the concentration and pH of the H2SO4 solution.mixing 17.5 mL of 4.700 M aluminum chloride with 24.0 mL of 2.00M silver (I) nitrate solution results in a precipitate. the resulting mixture contains a total free chloride ion concentration of
- Perform these calculations for nickel(II) carbonate. (a) With what volume of water must a precipitate containing NiCO3 be washed to dissolve 0.100 g of this compound? Assume that the wash water becomes saturated with NiCO3 (Ksp = 1.36 × 10–7).(b) If the NiCO3 were a contaminant in a sample of CoCO3 (Ksp = 1.0 × 10–12), what mass of CoCO3 would have been lost? Keep in mind that both NiCO3 and CoCO3 dissolve in the same solution.Why are many ionic precipitates washed with electrolyte solution instead of pure water?A sample is analyzed for chloride by the Volhard method. From the following data, calculate the percentage of chloride present:Weight of sample = 6.0000 g dissolved and diluted to 200 mLAliquot used = 25.00 mL AgNO3 added = 40.00ml of 0.1234MKSCN for back titration = 13.20ml of 0.0930M