Volhard method. A total of 50.00 ml of 0.1048M AgNO3 is added to the sample and 15.38 ml of 0.3116 M KSCN is required for the back titration. What is the weight % Cl- (molar mass 35.453)? Select the correct response: 2.5% 1.75% 2.2% 0.150% 3.5%
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- a) What mass of Fe(NH4)2(SO4)2•2H2O(s) is required to prepare a 500 mL solution containing 100 ppm (m:v) in Fe? b) Using this stock solution, what aliquot must be used to prepare calibration solutions, 100 mL volume, of the following concentrations: 0.100 ppm, 0.500 ppm, 2.00 ppm, 4.00 ppm, and 7.00 ppm.A student determined the concertration of NaOCI in a commercial bleach sample using the same technique described in section "F" of the Halogens and Their Compounds lab. The student required 18 drops of 0.01M Na25203 to reach the end point. What is the concentration (reported in percentage) of NaOCI in the bleach sample?3. Analysis of a mixture consisting of NaOH + Na2CO3 + inert matter gives the following data: 10.00 g. Its aqueous solution is diluted to 250.0 mL and two separate 25.00 mL sample portions are titrated. With one portion, an end point with phenolphthalein is obtained in cold solution, with 44.52 mL of 0.5000 N HCI. The other portion requires 46.53 mL of the acid for an end point with methyl orange. Calculate the percentage composition of the original sample.
- 1. A newly discovered iron ore was weighted (5.408 g) and worked up to produced 0.3785 g of ignited Fe2O3 precipitate. What is the percent purity of the iron in the sample? 2. Distinguish between equivalence point and end point.How many grams of Ag2CO3 will be soluble in 250 ml of 0.180 M AgNO3? (Ksp of Ag2CO3 = 5.95 x 10-10) Cr2O72- + 14 H+ + 6 e ----- 2 Cr3+ + 7H2O Eo = - 1.25 VMnO4- + 8 H+ + 5 e ---- Mn2+ + 4 H2O Eo = - 1.27 VFe3+ + e ------ Fe2+ Eo = - 1.20 VZn2+ + 2e --------- Zn Eo = - 0.76 V ( R = 0.08205 L.atm/mol.K; R = 8.314 J/mol.K; F = 96481 C/mol electron) ΔG = ΔH – TΔS ; E = Eo - 0.0257 ln Q ; ΔG = ΔGo + RT ln QCalculate the gravimetric factor of the following. 2 Fe3O4 is sought(Analyte), 3 Fe2O3 is weighed (Precipitate)
- Prepare 1.0 L of a 50.00 ppm iron solution from the solid Fe(NH4)2(SO4)2 of the80.0% purity. Clearly describe how to prepare this solution. If doneChlorimetric iron analysis using the calibration curve method, specify theform of preparation of 100.0 ml of each of the following standard solutions withcontents of 1.00, 5.00, 15.00 and 20.00 ppm of Fe respectively from the solutionmother (It suppose that the answers are: 0.3180, 2.00, 10.00, 20.00, 30.00 and 40.00 ml of the mother solution and dilute exactly to 100.0 mL with deionized water)A STOCK SOLUTION containing 0.1581 g/L K2CrO4 was prepared.In order to make the CALIBRATION STANDARD, 5 ml of the STOCK was transferredinto a 50ml volumetric flask and then diluted with an appropriate solvent.Calculate:(a) The ppm of K2CrO4 in the CALIBRATION STANDARD.(b) The molarity of K2CrO4 in the CALIBRATION STANDARD. (c) Calculate the molar absorptivity of K2CrO4 (at 371.0 nm). Assume that Beer's Law isobeyed over this concentration range.At 371.0 nm, this CALIBRATION STANDARD in a cell of path length 1.00 cm gave a %T of 59.752.A 600.0 mg sample consisting of only CaC2O4and Mg C2O4is heated at 500oC converting the two salts to CaCO3and MgCO3. The sample weighs 465.0 mg. If the sample had been heated at 900oC where the products are CaO and MgO, what would the mixture of oxides weigh? Show the clear and complete solution
- A shipment of containing NaOH (40 g/mol) and Na2CO3 (106 g/mol) was declared to contain less than 10 % impurity. However, Noel is suspicious that the declared impurity is higher. Being the best and brightest employee of the year, Noel weighed 1.000 g sample, dissolved in 50.0 mL of distilled water and titrated with cold 0.5000 M HCl. With Phenolphthalein as indicator, the solution turns colorless after the addition of 30.00 mL of the acid. Methyl Orange is then added, and 5.00 mL more of the acid is required before this this indicator changes color. Calculate the following: a. Determine the volume of the acid to fully neutralize NaOH (final answer up to one decimal place) =One gram of sodium hydroxide (NaOH) is used to adjust the pH of an aqueous solution (200 gallons) thatcontains 10 lbs of finely ground rhodochrosite (MnCO3) ore. Does the NaOH raise or lower the solutionpH? What is the amount of NaOH added in lbs/ton? What is the molarity (mol/l) of the system? Assumingthe NaOH is completely soluble and the system is at room temperature, what is the solid-to-liquid ratio(wt%) of the system?Five drops of dichlorofluorescein have been added to a solution containing 0.800 g sample which required 25.30 mL of 0.100 M AgNO3. (c) Calculate the weight percent NaCl in the original sample.