What do the melting points of the 6 samples tell you about their relative purities?

Fundamentals Of Analytical Chemistry
9th Edition
ISBN:9781285640686
Author:Skoog
Publisher:Skoog
Chapter7: Statistical Data Treatment And Evaluation
Section: Chapter Questions
Problem 7.10QAP
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Excess H20 Added
Slow/Fast
Sample #
Starting Mass
Mass Recovered
М.Р.
(mL)
Crystallization
1
041869|120.0- 120:5
O.42349 119.8 -1203
0:32429|120.7-121:3
slow
2
0.5046g
fast
3
D4920g
0.49339
Slow
4
fast
). 37089 121.9 - 122.7
0:49109
D.3019g
122:0-122.7
10
slow
10
fast
0-3472g
1a१-122-१
Observations:
• The
in compan'son to
the fast cooling.
slow cooling had a
lower
vange
added, the nigher the
me Hing point
The
move
water that
was
Calculate the % recovery for each sample
= mass
after
x100
mass
before
#4) 0.37089
#1) 0.41869
O-4991g
83.871.
75.17%%
0.4933g
#5) 0.30199
0 49109
#2) 0.42349
0:50469
83.91%
61.49%0
#6) 0.3472g
6.50149
69.25%0
#3) 0.32429
O.49209
65.89%
%3D
Transcribed Image Text:Excess H20 Added Slow/Fast Sample # Starting Mass Mass Recovered М.Р. (mL) Crystallization 1 041869|120.0- 120:5 O.42349 119.8 -1203 0:32429|120.7-121:3 slow 2 0.5046g fast 3 D4920g 0.49339 Slow 4 fast ). 37089 121.9 - 122.7 0:49109 D.3019g 122:0-122.7 10 slow 10 fast 0-3472g 1a१-122-१ Observations: • The in compan'son to the fast cooling. slow cooling had a lower vange added, the nigher the me Hing point The move water that was Calculate the % recovery for each sample = mass after x100 mass before #4) 0.37089 #1) 0.41869 O-4991g 83.871. 75.17%% 0.4933g #5) 0.30199 0 49109 #2) 0.42349 0:50469 83.91% 61.49%0 #6) 0.3472g 6.50149 69.25%0 #3) 0.32429 O.49209 65.89% %3D
What do the melting points of the 6 samples tell you about their relative purities?
Transcribed Image Text:What do the melting points of the 6 samples tell you about their relative purities?
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