Which of the ff is not true about recrystallization? a. acetanalide recrystallized only at cold temp b. congo red stain is removed by using animal charcoal c. acetanalide can be dissolved in hot h20
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Which of the ff is not true about recrystallization?
a. acetanalide recrystallized only at cold temp
b. congo red stain is removed by using animal charcoal
c. acetanalide can be dissolved in hot h20
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- The key to a successful HPLC procedure is good sample separation which is represented by a clean peak for each individual compound. What should we do to ensure a good sample preparation? A. Use a column and a mobile phase with different polarity B. Use a column and a mobile phase with the same polarity C. Use a lower temperature higher than the mobile phase boiling point D. All of thoseSuppose a particular extraction proceeds with a distribution coefficient of 7.5 The mature consists of a certain amount of caffeine dissolved in 100 mL of water. a .How much caffone was originally used when 0.31 g of the organic compound was dissolved in water and 150 = L ether was used as extraction solvent b. How much was dissolved in ether?Neel’s unknown solid 1) dissolves in hot ethanol, 2) is essentially insoluble in hexane, and 3) is insoluble in cold water, but sparingly soluble in warm water. Outline a recrystallization procedure.
- outline a separation scheme for isolating pure aspirin. lab video: https://www.youtube.com/watch?v=Y4NMpO1xI8UExplain why it is needed to filter the solvent before introducing it to the HPLC system2 Suppose a particular extraction proceeds with a distribution coefficient of 7.5. The mixture consists of a certain amount of caffeine dissolved 100 mL of water a. How much caffeine was originally used when 0.31 g of the organic compound was dissolved in water and 150 mL ether was used as extraction solvent b. How much was dissolved in ether?
- 1.What is the significance when KD is either a small or large value? 2. Methyl alcohol and ethyl alcohol are poor extraction solvents. Why?3. What is the major disadvantage of using ether as an extracting solvent?Suppose you have an organic sample X that is somewhat soluble in water, even though it issomewhat more soluble in dichloromethane or ether solvents. But if you do a singleextraction, you get only 60% of your material to transfer from the water to the organic layer.How many “washes” would it take to extract over 90% of your organic material extracted fromthe water layer?Thin‑layer chromatography (TLC) can be used as a preliminary identification method for many amphetamine‑type stimulants (ATS). Using a 0.25 mm thick silica gel stationary phase and a 98.5:1.5 methanol:concentrated ammonia mobile phase, a spot was observed to have traveled 3.52 cm when the solvent front traveled 8.81 cm. What is the retardation factor (?F)for the compound that composes this spot?
- 31 and 32. pls help and show solution plsss1. Which of the following may cause an increase in the calculated percent recovery of the recrystallized benzoic acid? a.Adding too much solvent in the receiving flask during hot filtrationb.Using cold water in rinsing the residue from the flask during hot filtration c.Using fluted filter paper during hot filtrationd.Not adding animal charcoal to the solution2. Which set of reagents can confirm that sulfate ions are present in two unkown solutions? a.1.0 M NaOH and excess NH3 b.0.1 M Ba(NO3)2 and 0.01 M KMnO4 c.1.0 M NaOH and 0.1 M K2Zn3[Fe(CN)6]2d.0.1 M Ba(NO3)2 and 1.0 M CH3COOHWhy does Naphthalene elute last in 95 percent Polydimethylsilicone and 5% phenyl-methyl silicone gas chromotagraphy system as compared to phenol and toleune(where toluene elutes first than phenol)