You are tasked to obtain a solid product from your laboratory activity. To verify the identity of your solid product, you measured its melting point. The results shows that the material melted over a 23º C range. After the material had cooled, you measured the melting point of the same sample again and found that this time the solid had a sharp melting point at the temperature that is characteristic of the solid product. (a) Why were the two melting points different? (b) What was responsible for the change in this melting point?

Macroscale and Microscale Organic Experiments
7th Edition
ISBN:9781305577190
Author:Kenneth L. Williamson, Katherine M. Masters
Publisher:Kenneth L. Williamson, Katherine M. Masters
Chapter5: Distillation
Section: Chapter Questions
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You are tasked to obtain a solid product from your laboratory activity. To verify the identity of your solid product, you measured its melting point. The results shows that the material melted over a 23º C range. After the material had cooled, you measured the melting point of the same sample again and found that this time the solid had a sharp melting point at the temperature that is characteristic of the solid product. (a) Why were the two melting points different? (b) What was responsible for the change in this melting point?

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