Experiment 3 Freezing Point Depression

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University of Nebraska, Lincoln *

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109L

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Chemistry

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Feb 20, 2024

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docx

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4

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Experiment 3 Determination of Freezing Point Depression Constant Total Points: 51 Student’s Name: Adam Miller Lab Section: 804 Report Your report should include the following: Data Tables 1-3 Results Tables 4-8 Final Results Table ALL the graphs you constructed (13 pts) NOTE: You must show your work for all calculations; no work, no credit Data Tables Data Table 1 (5 pts) Mass of Test Tube 17.245g Total Mass of Test Tube and Solvent 18.235g Mass of Solvent .990g Name of Solvent Myristic Acid Combination Number 3 Data Table 2 (5 pts) Combination Number (solute/solvent): Combination 3 = Solute-Palmitic, Solvent-Myristic Trial Number Approximate Mass of Solute (g) Total Mass of Test Tube and Solvent (g) (from Trial #1) Total Mass of Test Tube, Solvent, and Solute Added (g) (measured from balance) Total Mass of Solute Added (g) (calculated) 2 0.02 18.235g 18.260g .025g 3 0.04 18.235g 18.290g .055g 4 0.06 18.235g 18.304g .069g 5 0.08 18.235g 18.320g .085g
Experiment 3 Determination of Freezing Point Depression Constant Total Points: 51 Data Table 3—My Group’s Combination (11 pts) Chart Name: Combination 3 = Solute-Palmitic, Solvent-Myristic Actual Mass of Solute (g) Determined Freezing Point (°C) (read from graph) Change in Freezing Point (°C) (calculated) Molality of Solution (m) (calculated) Freezing Point Depression Constant (°C/m) (calculated) 0 g (pure solvent) 53.5 °C .025g 51.2 °C 2.3 °C .0985m 23.35 °C/m .055g 49.0 °C 4.5 °C .2167m 20.77 °C/m .069g 48.7 °C 4.8 °C .2718m 17.66 °C/m .085g 48.5 °C 5 °C .3349m 14.93 °C/m Example Calculation for Molality and Freezing Point Depression Constant (4 pts) For .025g .025g / 256.4g = 9.75E-5 mol 2.3 °C = (1)(.0985m)K F 9.75E-5 mol / 9.9E-4 kg = .0985m K F = 23.35 °C/m Result Table 4 (2 pts) Chart Name: Combination 5 = Solute-Myristic, Solvent-Lauric Actual Mass of Solute (g) Determined Freezing Point (°C) (read from graph) Change in Freezing Point (°C) (calculated) Molality of Solution (m) (calculated) Freezing Point Depression Constant (°C/m) (calculated) 0 g (pure solvent) 43.1°C .019g 41.8°C 1.3°C .0831m 15.64°C/m .040g 40.4°C 2.7°C .1750m 15.43°C/m .061g 39.5°C 3.6°C .2668m 13.49°C/m .080g 38.7°C 4.4°C .3500m 12.57°C/m
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