Experiment 3 Freezing Point Depression
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Experiment 3
Determination of Freezing Point Depression Constant
Total Points: 51
Student’s Name:
Adam Miller
Lab Section: 804
Report
Your report should include the following:
Data Tables 1-3
Results Tables 4-8
Final Results Table
ALL the graphs you constructed (13 pts)
NOTE: You must show your work for all calculations; no work, no credit
Data Tables
Data Table 1 (5 pts)
Mass of Test Tube
17.245g
Total Mass of Test Tube and Solvent
18.235g Mass of Solvent
.990g
Name of Solvent
Myristic Acid
Combination Number
3
Data Table 2 (5 pts)
Combination Number (solute/solvent): Combination 3 = Solute-Palmitic, Solvent-Myristic
Trial Number
Approximate Mass of Solute (g)
Total Mass of Test Tube and Solvent (g) (from Trial #1)
Total Mass of Test Tube, Solvent, and Solute Added (g) (measured from balance)
Total Mass of Solute Added (g) (calculated)
2
0.02
18.235g
18.260g
.025g
3
0.04
18.235g
18.290g
.055g
4
0.06
18.235g
18.304g
.069g
5
0.08
18.235g
18.320g
.085g
Experiment 3
Determination of Freezing Point Depression Constant
Total Points: 51
Data Table 3—My Group’s Combination (11 pts)
Chart Name:
Combination 3 = Solute-Palmitic, Solvent-Myristic
Actual Mass of Solute (g)
Determined Freezing Point (°C)
(read from graph)
Change in Freezing Point (°C)
(calculated)
Molality of Solution (m) (calculated)
Freezing Point Depression Constant (°C/m) (calculated)
0 g (pure solvent)
53.5 °C
.025g
51.2 °C
2.3 °C
.0985m
23.35 °C/m
.055g
49.0 °C
4.5 °C
.2167m
20.77 °C/m
.069g
48.7 °C
4.8 °C
.2718m
17.66 °C/m
.085g
48.5 °C
5 °C
.3349m
14.93 °C/m
Example Calculation for Molality and Freezing Point Depression Constant (4 pts)
For .025g
.025g / 256.4g = 9.75E-5 mol
2.3 °C = (1)(.0985m)K
F
9.75E-5 mol / 9.9E-4 kg = .0985m
K
F
= 23.35 °C/m
Result Table 4 (2 pts)
Chart Name:
Combination 5 = Solute-Myristic, Solvent-Lauric
Actual Mass of Solute (g)
Determined Freezing Point (°C)
(read from graph)
Change in Freezing Point (°C)
(calculated)
Molality of Solution (m) (calculated)
Freezing Point Depression Constant (°C/m) (calculated)
0 g (pure solvent)
43.1°C
.019g
41.8°C
1.3°C
.0831m
15.64°C/m
.040g
40.4°C
2.7°C
.1750m
15.43°C/m
.061g
39.5°C
3.6°C
.2668m
13.49°C/m
.080g
38.7°C
4.4°C
.3500m
12.57°C/m
Experiment 3
Determination of Freezing Point Depression Constant
Total Points: 51
Result Table 5 (2 pts)
Chart Name:
Combination 6 = Solute-Palmitic, Solvent-Lauric
Actual Mass of Solute (g)
Determined Freezing Point (°C)
(read from graph)
Change in Freezing Point (°C)
(calculated)
Molality of Solution (m) (calculated)
Freezing Point Depression Constant (°C/m) (calculated)
0 g (pure solvent)
41.9°C
.019g
39.1°C
2.8°C
.0762m
36.75°C/m
.055g
37.7°C
4.2°C
.2205m
19.05°C/m
.069g
37.2°C
4.7°C
.2766m
16.99°C/m
.085g
36.8°C
5.1°C
.3407m
14.97°C/m
Result Table 6 (2 pts)
Chart Name:
Combination 2 = Solute-Myristic, Solvent-Palmitic
Actual Mass of Solute (g)
Determined Freezing Point (°C)
(read from graph)
Change in Freezing Point (°C)
(calculated)
Molality of Solution (m) (calculated)
Freezing Point Depression Constant (°C/m) (calculated)
0 g (pure solvent)
60.5°C
.020g
54.7°C
5.8°C
.0908m
63.88°C/m
.052g
57.1°C
3.4°C
.2362m
14.39°C/m
.066g
50.8°C
9.7°C
.2998m
32.35°C/m
.086g
48.1°C
12.4°C
.3906m
31.75°C/m
Result Table 7 (2 pts)
Chart Name:
Combination 4 = Solute-Lauric, Solvent-Myristic
Actual Mass of Solute (g)
Determined Freezing Point (°C)
(read from graph)
Change in Freezing Point (°C)
(calculated)
Molality of Solution (m) (calculated)
Freezing Point Depression Constant (°C/m) (calculated)
0 g (pure solvent)
53.0°C
.021g
51.5°C
1.5°C
.1060m
14.15°C/m
.041g
51.2°C
1.8°C
.2070m
8.696°C/m
.061g
50.6°C
2.4°C
.3079m
7.795°C/m
.082g
50°C
3.0°C
.4139m
7.248°C/m
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Experiment 3
Determination of Freezing Point Depression Constant
Total Points: 51
Result Table 8 (2 pts)
Chart Name:
Combination 1 = Solute-Lauric, Solvent-Palmitic
Actual Mass of Solute (g)
Determined Freezing Point (°C)
(read from graph)
Change in Freezing Point (°C)
(calculated)
Molality of Solution (m) (calculated)
Freezing Point Depression Constant (°C/m) (calculated)
0 g (pure solvent)
60.3°C
.018g
59.3°C
1.0°C
.0903m
11.07°C/m
.049g
58.8°C
1.5°C
.2458m
6.103°C/m
.069g
58.3°C
2.0°C
.3462m
5.777°C/m
.087g
57.3°C
3.0°C
.4365m
6.873°C/m
Final Results (3 pts)
Solvent
Average Freezing Point Depression Constant (°C/m)
Lauric Acid
18.11°C/m
Myristic Acid
14.32°C/m
Palmitic Acid
21.52°C/m
I added all 8 values for each solvent and then divided by 8.
NOTE: Average the values from all trials for each solvent.
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