101 Ex4 InlabnotesTemplate_2309

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University of Victoria *

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101

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Chemistry

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Feb 20, 2024

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docx

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Uploaded by LieutenantDeer3412

Chem 101 Laboratory Exercise #4 Laboratory Notebook Spectrophtometric determination of Salicylic Acid Using Microsoft Word, students are to write their in-lab notes below while completing the Laboratory exercise. The Laboratory notebook must be uploaded to the CHEM 101 Lab Brightspace site as a readable .pdf by the end of the lab period. Please see page 7 of the 202309 CHEM 101 lab manual as to all the information required in the in-lab notes. The documentation below must reflect the student’s own work without assistance from others. Name: Lab Section: Quad: Date: In-lab Notes: Get 25mL of stock iron solution in a 100mL beaker. Put 5mL of stock iron solution into each of the four 25mL flasks. Get 30mL of stock salicylic acid solution. Use a pipet to add 1mL of salicylic acid to flask #1 (clear light purple color). Use a pipet to add 5mL of salicylic acid to flask #2 (dark purple that is semi-transparent). Use a pipet to add 10mL of salicylic acid to flask #3 (extremely dark purple that is no longer transparent). Add distilled water to all four flasks, fill to the line (clear solution). Get a new 25mL flask and add 0.3mL of acne cleanser, 5mL of iron solution, and fill the rest with distilled water (extremely dark purple similar to flask #3). Get the absorbance of each flask. Measurements: Stock iron nitrate solution concentration = 0.010M Stock salicylic acid solution concentration = 0.002917M Commercial product used: Clean & Clear blackhead cleaning astringent. Johnson & Johnson, Markham, Ontario, L3R 5L2, 0038C. Commercial product is 1% salicylic acid
Blank flask (#4) Flask #1 Flask #2 Flask #3 Unknown flask Stock iron solution 5.00mL 5.00mL 5.00mL 5.00mL 5.00mL Stock salicylic solution 0.0 1.00mL 5.00ml 10.00mL - Acne cleanser - - - - 0.3mL absorbance 0 0.090 0.244 0.831 1.390 1.488 1.196 1.207 1.189
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