Lab Report: Calibration of Volumetric Glassware Essay

In this lab experiment our main focus was to get skillful in using tools such as the metric ruler, balances, thermometer, and graduated cylinder to capture measurements of length, mass, temperature and volume. Additionally, this lab helped us to become more familiar with the uncertainty of measurements, as well as becoming efficient with rounding our measurements to the correct numbers of significant figures. Our results are measured consistently with rounding to the closest answer we could possibly acquire as the data can tell you.

because each of the objects displaced the water by 1 mL, their mass over that mL is their density.

First, I will get my materials and set up the scale and 10 mL cylinder and refraction cell. I will check the size of the graduated cylinder to find out the volume. (LxHxW) That will equal 40.5mL for volume. I will see how much the cell weighs alone, and then I will 0 out the scale to see how much the water weighs. Then I will see how much the water and the cell weigh together. I will do this for the cell and cylinder. I will check to see if the density I calculated is what it is supposed to be at 1.00.

m = mass of water = density x volume = 1 x 26 = 26 grams

The measuring cylinder was then used to accurately measure out 20 mL of water, which was then poured into the test tube that would be used for the experiment. The test tube was then placed into the clamp, which was then adjusted in order to make sure that the test tube was grasped firmly and would not fall out.

E. What would happen if you dropped the object into the beaker while using the Archimedes’ Principle method instead of submerging the object?

Abstract: This experiment introduced the student to lab techniques and measurements. It started with measuring length. An example of this would be the length of a nickel, which is 2cm. The next part of the experiment was measuring temperature. I found that water boils around 95ºC at 6600ft. Ice also has a significant effect on the temperature of water from the tap. Ice dropped the temperature about 15ºC. Volumetric measurements were the basis of the 3rd part of the experiment. It was displayed during this experiment that a pipet holds about 4mL and that there are approximately 27 drops/mL from a short stem pipet. Part 4 introduced the student to measuring

Procedure: I used a ruler, thermometer, and scale to take measurements. I used a graduated cylinder, short step pipet, scale, and ruler to determine volume and density. I used a volumetric flask, graduated pipet, pipet bulb, scale, and glass beaker to determine concentrations and densities of various dilutions.

To achieve a good volumetric technique, the experimenter needs to be able to correctly complete certain procedures.

The volume of a small test tube and a thin-stemmed pipet were determined in this section of the lab. Water was poured into a small test tube until the water reached the very top edge of the test tube. The test tube was then emptied into a plastic 25 mL graduated cylinder and volume was measured and recorded into data table 3. A think-stemmed pipet was completely filled with water. Drops were carefully counted and emptied into the empty plastic 25 mL graduated cylinder until the water level reached 1 mL. The number of drops in 1 mL was recorded into data table 3. The thin-stemmed pipet had a total volume of 4 mL and that was also recorded into data table 3.

Abstract: The objective of the lab is to determine the volumes of the polystyrene spheres with three different measuring tools: Water Displacement, Analytical Scale, and Triple Beam Balance Scale. The experiment is meant to help understand the concept and application of precision and accuracy in experimental measurements. Accuracy is a measure of how closely the results of repeated measurements are to the true value of what is being measured. Precision is the variability in the results from the repeated measurements, and how close the repeated measurements were to one another. In this lab, the method for measuring the volume of the polystyrene spheres is done with the previously stated tools: Water Displacement, Analytical Scale, and Triple Beam Balance Scale. The standard deviation for the entire classes volumes and masses are recorded to determine the densities.

3. The volume of a fixed mass of a liquid sample increases as the temperature rises from 20 to

In order to minimize errors and to "place" the solutions in the same environment, the same volume should be extracted from each solution using the syringes.

In the third stage of this experiment, the density of a liquid was determined and compared to known standards. A 100ml beaker was filled to about half-full with room-temperature distilled water. The temperature of the water in ◦C was recorded in order to compare to known standards later. A 50ml beaker was then weighed on a scale in order to determine mass and recorded. A sample of the distilled water with an exact volume of 10ml was then placed in the 50ml beaker using a volumetric pipette. The 50ml beaker with the 10ml of water was then weighed again and the initial mass of the beaker was subtracted from this mass to obtain the mass of the 10ml of water. With the volume and the mass of the water now known, density was calculated using d = m/V and recorded in g/ml. This process was then repeated to check for precision and compared to standard values to check for accuracy. Standard values were obtained from CRC Handbook, 88th Ed.

For this experiment setup, following materials are needed such as a Kundt's tube apparatus, a meter stick, a piece of cloth, a thermometer,