ll SuperNet ?09:2767%A moodle.unizwa.edu.om2- Heat Decomposition mass Curve of sample M with mass 3.335 mg is shown below.Study the TGA thermogram and answer the following questions: -1201.846%A100 -28.23%80B20.28%10.84%40D20-200300400600700800Temperature ("C)a- Calculate the total amount of mass loss in mg of the sample at steps1- A2- Bb- How much the residue of the sample in mg after the heat decomposition hascompleted?II

Given, The mass of the sample = 3.335 mg. The weight loss after A decomposition = 1.846 % The weight…

2- Heat Decomposition mass Curve of sample M with mass 3.335 mg is shown below. Study the TGA thermogram and answer the following questions: - 1.846% A 100 28.23% B 20.28% 10.84% D 200 400 s00 600 700 800 Temperature ("C) a- Calculate the total amount of mass loss in mg of the sample at steps 1- A 2- B b- How much the residue of the sample in mg after the heat decomposition has completed?

2- Heat Decomposition mass Curve of sample M with mass 3.335 mg is shown below. Study the TGA thermogram and answer the following questions: - 1.846% A 100 28.23% B 20.28% 10.84% D 200 400 s00 600 700 800 Temperature ("C) a- Calculate the total amount of mass loss in mg of the sample at steps 1- A 2- B b- How much the residue of the sample in mg after the heat decomposition has completed?

Principles of Instrumental Analysis

7th Edition

ISBN:9781305577213

Author:Douglas A. Skoog, F. James Holler, Stanley R. Crouch

Publisher:Douglas A. Skoog, F. James Holler, Stanley R. Crouch

Chapter33: Automated Methods Of Analysis

Section: Chapter Questions

Problem 33.8QAP

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For Indirect Iodometric Analysis of Copper... ~0.0896g KIO3 necessary to consume 350mL of 0.1 M Na2S2O3, Na2S2O3 is stored in an amber glass bottle until ready for use. Primary Standard KIO3 has 2g of KI, 50mL of DI water, and 10 mL of 1.0M HCl is added then immediately titrated with Na2S2O3 until medium yellow or straw... then 5mL of starch indicator is added and titrated again until blue black color turns clear. Unknown CuO use 1.2G of Unknown, 20mL of HNO3 heated until sample dissolved, 25 mL of DI water added and boiled until clear light blue color, after cooling 1:1 NH3 added (~34.47 mL of NH4OH reagent) until permanent deep blue color amine complex, 2g of NH4HF2 added and swirled until dissolved, 3 g of KI is added then titrated immediately with Na2S2O3 until brown color of iodide is nearly gone (brown milk color), 2 g of KSCN and 3 mL of starch indicator is then added with titration continuing until disappearance of new blue black color. 1. Na2CO3 is often added to thiosulfate…
For Indirect Iodometric Analysis of Copper... ~0.0896g KIO3 necessary to consume 350mL of 0.1 M Na2S2O3, Na2S2O3 is stored in an amber glass bottle until ready for use. Primary Standard KIO3 has 2g of KI, 50mL of DI water, and 10 mL of 1.0M HCl is added then immediately titrated with Na2S2O3 until medium yellow or straw... then 5mL of starch indicator is added and titrated again until blue black color turns clear. Unknown CuO use 1.2G of Unknown, 20mL of HNO3 heated until sample dissolved, 25 mL of DI water added and boiled until clear light blue color, after cooling 1:1 NH3 added (~34.47 mL of NH4OH reagent) until permanent deep blue color amine complex, 2g of NH4HF2 added and swirled until dissolved, 3 g of KI is added then titrated immediately with Na2S2O3 until brown color of iodide is nearly gone (brown milk color), 2 g of KSCN and 3 mL of starch indicator is then added with titration continuing until disappearance of new blue black color. 4. Why is the starch indicator solution…
Procedure: analytically transfer between 0.4053g of iron(III) chloride hexahydrate, FeCl 3•6 H2O (M = 270.2957g•mol-1), and dissolve in 5.5 mL distilled, deionized water. Support the tube on a stir plate and over a 15-minute period add, using the 10mL burette, 5mL of a nominal 600mM solution of 2,4 pentandione in methanol under constant stirring. To the resulting solution, add via a 10mL burette 3mL of a nominal 450mM sodium acetate solution stirring constantly. At this point, a red crystalline solid should begin to precipitate. Transfer and support the reaction vessel in the hot water bath and once the reaction mixture has reached a stable temperature in the desired range, maintain the reaction mixture at this temperature, under constant stirring, for a 15-minute period Initial weight of iron(III) chloride hexahydrate: 0.4053g The final weight of the reaction tris(acetylacetonate)iron(III): 19.6 mg 3. What is the charge on the metal in the starting material for your synthesized…
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