b) The thermogravimetric curve for calcium salicylate monohydrate (CAC14H1006-H2O) is shown below. (mw 332 g/mol). Starting with an initial sample mass of 16.55 mg, calculate the mass of the sample remaining when it is heated to i) 350 oc and ii) 800 oc. The first step is loss Of H20 (mw 18 g/mol), followed by loss Of C703H6 (mw 138 g/mol), then C6H4 (mw 76 g/mol) and finally C02 (mw 44 g/mol). Give your answers to two decimal places and show your work. CaC,,H06 H,O CaC,,H,0 20- 40 CaC,0,H, 60 CaCO, CaO 80 100 200 800 Temperature ("C) 400 600 1000 Mass loss (%)

Fundamentals Of Analytical Chemistry
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ISBN:9781285640686
Author:Skoog
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Chapter31: Introduction To Analytical Separations
Section: Chapter Questions
Problem 31.19QAP
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b) The thermogravimetric curve for calcium salicylate monohydrate (CaC14H1006-H20) is shown
below. (mw 332 g/mol). Starting with an initial sample mass of 16.55 mg, calculate the mass of the
sample remaining when it is heated to ) 350 oc and ii) 800 oc.
The first step is loss Of H20 (mw 18 g/mol), followed by loss Of C703H6 (mw 138 g/mol), then C6H4
(mw 76 g/mol) and finally CO2 (mw 44 g/mol). Give your answers to two decimal places and show
your work.
CaC,,HO, H.O
CaC.,H,0
of
20-
40
CaC,0.H,
60-
CACO,
CaO
80
100
200 400 600 800 100
Temperature (C)
Transcribed Image Text:b) The thermogravimetric curve for calcium salicylate monohydrate (CaC14H1006-H20) is shown below. (mw 332 g/mol). Starting with an initial sample mass of 16.55 mg, calculate the mass of the sample remaining when it is heated to ) 350 oc and ii) 800 oc. The first step is loss Of H20 (mw 18 g/mol), followed by loss Of C703H6 (mw 138 g/mol), then C6H4 (mw 76 g/mol) and finally CO2 (mw 44 g/mol). Give your answers to two decimal places and show your work. CaC,,HO, H.O CaC.,H,0 of 20- 40 CaC,0.H, 60- CACO, CaO 80 100 200 400 600 800 100 Temperature (C)
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