A 60.0 mL solution of 0.0450 M hydroxylamine is extracted with 125 mL of solvent. The distribution constant for the reaction is 5.00 and the pK, of the protonated form of hydroxylamine is 5.960. Calculate the concentration of hydroxylamine remaining in the aqueous phase at pH = 4.50 and pH = 6.50. [hydroxylamine] at pH = 4.50: M [hydroxylamine] at pH = 6.50: M
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- An analysis for borohydride ion is based on its reaction with Ag+: BH4- + 8Ag+ + 8OH- → H2BO3- + 8Ag(s) + 5H2O The purity of a quantity of KBH4 to be used in an organic synthesis was established by diluting 3.258g of the material to exactly 500.0mL, treating a 100.0 mL aliquot with 50.00 mL of 0.2639M AgNO3 and titrating the excess silver ion with 3.36 mL of 0.0397 M KSCN. Calculate the percent purity of the KBH4 [Report the numerical value of the result to two decimal places - NO UNITS]A 0.703 g sample of a commercial detergent was red-calcined to destroy its components. organic. Treatment of the residue with hot HCl gave phosphorus in solution as H3PO4. the phosphate was precipitated as MgNH4PO4-6H2O by the addition of Mg + 2 or followed by aqueous NH3. The precipitate was filtered, washed, and converted to Mg2P2O7 by calcination at 1000 C. The residue weighed 0.432 g. Calculate the percentage of phosphorus in the sample.Suppose your colleague was relying on receiving your purified product in order to prepare a dilute aqueous standard solution of benzoic acid e.g. for a titration. She takes 160 mg of your benzoic acid and dissolves it in just enough water so the solution exactly fills a 250 mL volumetric flask. Given that the acid dissociation constant of benzoic acid Ka = 6.3 x 10-5, calculate the pH of her resulting solution.
- What weight of strontium acetate containing 99% Sr(CH3COOH)2.½H2O must be used as sample in an assay according to the general method for alkali salts of organic acids if, after treatment of the ash with 50.00 ml of 0.5162 N hydrochloric acid, it is desirable to consume 30.00 ml of 0.4675 N sodium hydroxide in the back titration?A biochemical reaction takes place in a 1.00 ml solution of 0.0250 Mphosphate buffer initially at pH = 7.20 (as shown for pKas of phosphatespecies).(a) Are the concentrations of any of the four possible phosphate speciesnegligible? If so, identify them and explain your answer.(b) During the reaction, 3.80 μmol of HCl are produced. Calculate the finalpH of the reaction solution. Assume that the HCl is completely neutralizedby the buffer.0.641 g of a semi-synthetic alkaloid was dissolved in 25 ml of 1% w/v acetic acid and wasanalysed directly by HPLC. The solution was found to contain 1.42 mg/100 ml of an impurity.What is the level of impurity in % w/w and ppm? Calculate the pH of a buffer system made by dissolving 1.2 g of acetic acid and 0.82 g ofsodium acetate in 500 ml of distilled water (pKa of acetic acid = 4.7)
- Using the reagents, prepare 100mL solution with a concentration of 25.0 mM Tris buffer at a final pH of 7.70. •Solid Tris, FW = 121.1• Solid Tris-C1, the conjugate acid of Tris. It has a pKa of 8.30 (at 25° C) and a FW of 157.6. •deionized waterThe pKb of the organic base nicotine (denoted Nic) is 5.98. Write the corresponding protonation reaction, the deprotonation reaction of the conjugate acid, and the value of pKa for nicotine.John wanted to determine the protein content of his blood. To do so, he obtained 1.00 mLof blood, and diluted it to 10.00 mL. From that solution, he subjected 1.00 mL to Kjeldahl analysis. After digestion, the liberated NH3 was distilled in a flask containing exactly 25.00 mL of 0.0150 M H3BO3. Titration requires 5.85 mL of standard 0.0150 M NaOH to reach the desired endpoint. If a typical blood sample contains 15.45 g N per 100 g protein, calculatethe protein content (in g/mL) in the sample of John’s blood.
- What are the concentrations of the various ionic species in a 0.1M solution of lysine at pH 4, 7, and 10?The measured pH of a 0.100 M solution of triethylamine (NEt3) is 11.68. What pKa of triethylammonium (HNEt3+) is implied by this data? Enter your response to the nearest 0.01.John wanted to determine the protein content of his blood. To do so, he obtained 1.00 mL of blood, and diluted it to 10.00 mL. From that solution, he subjected 1.00 mL to Kjeldahl analysis. After digestion, the liberated NH3 was distilled in a flask containing exactly 25.00 mL of 0.0150 M H3BO3. Titration requires 5.85 mL of standard 0.0150 M NaOH to reach the desired endpoint. If a typical blood sample contains 15.45 g N per 100 g protein, calculate the protein content (in g/mL) in the sample of John’s blood.