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Calculate the average and standard deviations for each solution (and solvent).
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- How to prepare the solutions listed below Solution 1) 25 mL 7 M sulfuric acid and the respective dilution of this solution to prepare 50 mL 2 M sulfuric acid in deionised water. Sulfuric acid Mw = 98.079 g mol-1 Sulfuric acid density = 1.84 g mL-1 Sulfuric acid purity = 98% Solution 2) 100 mL 0.02M potassium permanganate potassium permanganate Mw = 158.03 g mol-1 potassium permanganate purity = 99%Melting point: 122-123 experimental product melting point: 120 mass of starting material: 1.04 mass of product: 0.85g what is limiting reagent and percent yield?The following reaction is carried out with [PCl5]i = 0.400 M at 25 °C. PCl5(g) ⇌ PCl3(g) + Cl2(g) K=0.00105 Use the small x approximation and “test x”. Report the percent (to two decimal places) when testing x.
- Using the percent purity calculations, determine the percent yield of synthesis of aspirin. Part I Synthesis of Aspirin Mass of salicylic acid used (g) 2.029g Volume of acetic anhydride used (mL) 5ml Mass of acetic anhydride used (vol. × 1.08 g/mL) 5.4g Mass of aspirin synthesized (g) 3.256g Part II Melting Temperature Data Melting temperature (°C) 133°C Part III Salicylic Acid Standard Stock Solution Initial mass of salicylic acid (g) 0.210g Moles of salicylic acid (mol) 0.0147 mol Initial molarity of salicylic acid (M) 0.724 M Part III Beer’s Law Data for Salicylic Acid Standard Solutions Trial Concentration (M) Absorbance Water (mL) 1 10 0.301 0 2 7.5 0.219 2.5 3 5.0 0.163 5.0 4 2.5 0.074 7.5 Best-fit line equation for the salicylic acid standards Test of the Purity of the Synthesized Aspirin Initial mass of aliquot of product (g)…1 Report on how to decrease the droplet evaporation time for liquidfuel combustion.Calculate the Constant Weight (in grams) of the Empty Crucibles. Show your solution. Crucible No. 1 2 3 Weighing 1 22.6035 22.0223 24.1535 Weighing 2 22.6017 22.0204 24.1533 Weighing 3 22.5994 22.0199 - Weighing 4 22.5992 - - Constant Weight, g ??? ??? ???
- Use E5C.1(a) to Plot the data in excel. Place two data sets on the same graph: one for temp vs. x and one for temp vs y (remember, x and y are the mole fractions and they belong on the x-axis). Don’t forget to include the boiling points of the pure substances – they are data, too. Add a trendline (polynomial, 3rd order should work) to each of the coexistence lines separately. Scale the plot appropriately and use the graph to answer the questions. Then complete E5C.1(b)Concentration of AR Stock Solution (ppmppm) 21.22 Unrounded Rounded Concentration of AR Stock Solution (μMμM) 42.7461 42.7What is ΔSsurr for a reaction at 28.6 °C with ΔHsys = 38.9 kJ mol-1 ? Express your answer in J mol-1 K-1 to at least two significant figures.
- Detailed calculations on how to prepare the solutions listed below Solution: 50 mL 1 M oxalic acid Oxalic acid Mw = 90.03 g mol-1 Oxalic acid purity = 98% Solution: 10 mL 3 M sulfuric acid Sulfuric acid Mw = 98.079 g mol-1 Sulfuric acid density = 1.84 g mL-1 Sulfuric acid purity = 98% Solution: 10 mL saturated potassium oxalate potassium oxalate (monohydrate used) Mw = 184.23 g mol-1 Solubility of potassium oxalate in water at 25°C = 360 mg mL-1 Solution :20 mL 3% hydrogen peroxide Hydrogen peroxide is commercially available as a 32% solution.DATA Note: Use the videos as references except when data is provided here. Table 1. Selection of Recrystallizing Solvent. Solvents Dissolution at room temperature? (+ or −) Dissolution at elevated temperature? (+ or −) Distilled water - - Acetone + n/a 95% ethanol - + Toluene + n/a Solid sample: Naphthalene Table 2. Mass Measurements. Mass, g Sample solid 0.5021 Empty watch glass 35.7602 Watch glass with recrystallized sample 36.2485 Table 3. Melting Point Determination. Temperature, oC Appearance of Sample in Capillary Tube … Solid 78.4 Solid 79.3 Solid with signs of liquid 79.9 Solid, liquid 80.6 Liquid, solid 81.3 Liquid with signs of solid … Liquid Theoretical Melting Point, oC: 80.2°C (176.4°F) QUESTIONS Which solvent should be used as the recrystallizing solvent? Check if your chosen solvent satisfies all characteristics of a good…100.0 cm3 of a 1.234 mol.dm-3 solution of nickel(II) nitrate was added to 150.0 cm3 of a 1.178 mol.dm-3 solution of sodium carbonate. Determine the limiting reagent